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1-(4-Chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone

In the title compound, C(13)H(15)ClN(2)O, there are two crystallographically independent but conformationally similar (E)-mol­ecules in the asymmetric unit [dihedral angles between the phenyl ring and a common planar fragment of the 1,3-diazepane moiety = 47.34 (16) and 48.00 (16)°]. The seven-membe...

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Autores principales: Zhang, Xiao-Wei, Xia, Jian-Hui, Xu, Zhao-Hui, Wang, Li-Ben, Yu, Chu-Yi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3685108/
https://www.ncbi.nlm.nih.gov/pubmed/23795127
http://dx.doi.org/10.1107/S1600536813013858
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author Zhang, Xiao-Wei
Xia, Jian-Hui
Xu, Zhao-Hui
Wang, Li-Ben
Yu, Chu-Yi
author_facet Zhang, Xiao-Wei
Xia, Jian-Hui
Xu, Zhao-Hui
Wang, Li-Ben
Yu, Chu-Yi
author_sort Zhang, Xiao-Wei
collection PubMed
description In the title compound, C(13)H(15)ClN(2)O, there are two crystallographically independent but conformationally similar (E)-mol­ecules in the asymmetric unit [dihedral angles between the phenyl ring and a common planar fragment of the 1,3-diazepane moiety = 47.34 (16) and 48.00 (16)°]. The seven-membered ring system adopts a chair conformation in both molecules. In the crystal, N—H⋯O hydrogen bonds lead to chains extending along the b-axis direction.
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spelling pubmed-36851082013-06-21 1-(4-Chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone Zhang, Xiao-Wei Xia, Jian-Hui Xu, Zhao-Hui Wang, Li-Ben Yu, Chu-Yi Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(15)ClN(2)O, there are two crystallographically independent but conformationally similar (E)-mol­ecules in the asymmetric unit [dihedral angles between the phenyl ring and a common planar fragment of the 1,3-diazepane moiety = 47.34 (16) and 48.00 (16)°]. The seven-membered ring system adopts a chair conformation in both molecules. In the crystal, N—H⋯O hydrogen bonds lead to chains extending along the b-axis direction. International Union of Crystallography 2013-05-25 /pmc/articles/PMC3685108/ /pubmed/23795127 http://dx.doi.org/10.1107/S1600536813013858 Text en © Zhang et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Xiao-Wei
Xia, Jian-Hui
Xu, Zhao-Hui
Wang, Li-Ben
Yu, Chu-Yi
1-(4-Chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone
title 1-(4-Chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone
title_full 1-(4-Chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone
title_fullStr 1-(4-Chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone
title_full_unstemmed 1-(4-Chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone
title_short 1-(4-Chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone
title_sort 1-(4-chloro­phen­yl)-2-(1,3-diazepan-2-yl­idene)ethanone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3685108/
https://www.ncbi.nlm.nih.gov/pubmed/23795127
http://dx.doi.org/10.1107/S1600536813013858
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