Cargando…
Microwave-Assisted Hydrogenation of Codeine in Aqueous Media
An efficient one-pot microwave-assisted hydrogenation of codeine was achieved in aqueous solution. This technique is simple, fast, environmentally friendly, and highly efficient. Structure of produced dihydrocodeine was approved by using FT-IR, (1)H NMR, (13)C NMR, EIMS, and elemental analysis techn...
Autores principales: | , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Scholarly Research Network
2012
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3767335/ https://www.ncbi.nlm.nih.gov/pubmed/24052836 http://dx.doi.org/10.5402/2012/104975 |
_version_ | 1782283651206086656 |
---|---|
author | Taktak, F. Bulduk, I. |
author_facet | Taktak, F. Bulduk, I. |
author_sort | Taktak, F. |
collection | PubMed |
description | An efficient one-pot microwave-assisted hydrogenation of codeine was achieved in aqueous solution. This technique is simple, fast, environmentally friendly, and highly efficient. Structure of produced dihydrocodeine was approved by using FT-IR, (1)H NMR, (13)C NMR, EIMS, and elemental analysis technique. Its purity analysis was performed by using HPLC and assay analysis was performed by using potentiometric titration methods. |
format | Online Article Text |
id | pubmed-3767335 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | International Scholarly Research Network |
record_format | MEDLINE/PubMed |
spelling | pubmed-37673352013-09-19 Microwave-Assisted Hydrogenation of Codeine in Aqueous Media Taktak, F. Bulduk, I. ISRN Org Chem Research Article An efficient one-pot microwave-assisted hydrogenation of codeine was achieved in aqueous solution. This technique is simple, fast, environmentally friendly, and highly efficient. Structure of produced dihydrocodeine was approved by using FT-IR, (1)H NMR, (13)C NMR, EIMS, and elemental analysis technique. Its purity analysis was performed by using HPLC and assay analysis was performed by using potentiometric titration methods. International Scholarly Research Network 2012-09-20 /pmc/articles/PMC3767335/ /pubmed/24052836 http://dx.doi.org/10.5402/2012/104975 Text en Copyright © 2012 F. Taktak and I. Bulduk. https://creativecommons.org/licenses/by/3.0/ This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. |
spellingShingle | Research Article Taktak, F. Bulduk, I. Microwave-Assisted Hydrogenation of Codeine in Aqueous Media |
title | Microwave-Assisted Hydrogenation of Codeine in Aqueous Media |
title_full | Microwave-Assisted Hydrogenation of Codeine in Aqueous Media |
title_fullStr | Microwave-Assisted Hydrogenation of Codeine in Aqueous Media |
title_full_unstemmed | Microwave-Assisted Hydrogenation of Codeine in Aqueous Media |
title_short | Microwave-Assisted Hydrogenation of Codeine in Aqueous Media |
title_sort | microwave-assisted hydrogenation of codeine in aqueous media |
topic | Research Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3767335/ https://www.ncbi.nlm.nih.gov/pubmed/24052836 http://dx.doi.org/10.5402/2012/104975 |
work_keys_str_mv | AT taktakf microwaveassistedhydrogenationofcodeineinaqueousmedia AT bulduki microwaveassistedhydrogenationofcodeineinaqueousmedia |