An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl(3)-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst

A new BiCl(3)-loaded montmorillonite K10 catalyst has been prepared by solid dispersion method and was characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and cyclic voltammetry (CV) measurements. BiCl(3) loaded K10 (BiCl(3)-K10) has been used as solid aci...

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Detalles Bibliográficos
Autores principales: Ravi, K., Krishnakumar, B., Swaminathan, M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Scholarly Research Network 2012
Materias:
Research Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3767373/
https://www.ncbi.nlm.nih.gov/pubmed/24052847
http://dx.doi.org/10.5402/2012/595868
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author Ravi, K.
Krishnakumar, B.
Swaminathan, M.
author_facet Ravi, K.
Krishnakumar, B.
Swaminathan, M.
author_sort Ravi, K.
collection PubMed
description A new BiCl(3)-loaded montmorillonite K10 catalyst has been prepared by solid dispersion method and was characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and cyclic voltammetry (CV) measurements. BiCl(3) loaded K10 (BiCl(3)-K10) has been used as solid acid catalyst for the synthesis of azine derivatives from benzophenone hydrazone and ketones/aldehydes by simple physical grinding. This BiCl(3)-K10 gives an excellent yield with short reaction time and is an inexpensive, easily recyclable catalyst for this reaction.
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spelling pubmed-37673732013-09-19 An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl(3)-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst Ravi, K. Krishnakumar, B. Swaminathan, M. ISRN Org Chem Research Article A new BiCl(3)-loaded montmorillonite K10 catalyst has been prepared by solid dispersion method and was characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and cyclic voltammetry (CV) measurements. BiCl(3) loaded K10 (BiCl(3)-K10) has been used as solid acid catalyst for the synthesis of azine derivatives from benzophenone hydrazone and ketones/aldehydes by simple physical grinding. This BiCl(3)-K10 gives an excellent yield with short reaction time and is an inexpensive, easily recyclable catalyst for this reaction. International Scholarly Research Network 2012-10-08 /pmc/articles/PMC3767373/ /pubmed/24052847 http://dx.doi.org/10.5402/2012/595868 Text en Copyright © 2012 K. Ravi et al. https://creativecommons.org/licenses/by/3.0/ This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Research Article
Ravi, K.
Krishnakumar, B.
Swaminathan, M.
An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl(3)-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst
title An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl(3)-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst
title_full An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl(3)-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst
title_fullStr An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl(3)-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst
title_full_unstemmed An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl(3)-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst
title_short An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl(3)-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst
title_sort efficient protocol for the green and solvent-free synthesis of azine derivatives at room temperature using bicl(3)-loaded montmorillonite k10 as a new recyclable heterogeneous catalyst
topic Research Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3767373/
https://www.ncbi.nlm.nih.gov/pubmed/24052847
http://dx.doi.org/10.5402/2012/595868
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