Methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate

In the title compound, C(18)H(15)N(3)O(5)S, the approximately planar quinazoline ring system [maximum deviation = 0.097 (3) Å] forms a dihedral angle of 76.53 (19)° with the phenyl ring. The terminal -C(=O)—O—C group is disordered over two sets of sites with a site-occupancy ratio of 0.811 (17):0.18...

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Autores principales: Al-Suwaidan, Ibrahim A., Abdel-Aziz, Alaa A.-M., El-Azab, Adel S., Chidan Kumar, C. S., Fun, Hoong-Kun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3770384/
https://www.ncbi.nlm.nih.gov/pubmed/24046669
http://dx.doi.org/10.1107/S1600536813016127
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author Al-Suwaidan, Ibrahim A.
Abdel-Aziz, Alaa A.-M.
El-Azab, Adel S.
Chidan Kumar, C. S.
Fun, Hoong-Kun
author_facet Al-Suwaidan, Ibrahim A.
Abdel-Aziz, Alaa A.-M.
El-Azab, Adel S.
Chidan Kumar, C. S.
Fun, Hoong-Kun
author_sort Al-Suwaidan, Ibrahim A.
collection PubMed
description In the title compound, C(18)H(15)N(3)O(5)S, the approximately planar quinazoline ring system [maximum deviation = 0.097 (3) Å] forms a dihedral angle of 76.53 (19)° with the phenyl ring. The terminal -C(=O)—O—C group is disordered over two sets of sites with a site-occupancy ratio of 0.811 (17):0.189 (17). In the crystal, mol­ecules are linked via weak C—H⋯O hydrogen bonds into sheets parallel to the ac plane.
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spelling pubmed-37703842013-09-17 Methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate Al-Suwaidan, Ibrahim A. Abdel-Aziz, Alaa A.-M. El-Azab, Adel S. Chidan Kumar, C. S. Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(18)H(15)N(3)O(5)S, the approximately planar quinazoline ring system [maximum deviation = 0.097 (3) Å] forms a dihedral angle of 76.53 (19)° with the phenyl ring. The terminal -C(=O)—O—C group is disordered over two sets of sites with a site-occupancy ratio of 0.811 (17):0.189 (17). In the crystal, mol­ecules are linked via weak C—H⋯O hydrogen bonds into sheets parallel to the ac plane. International Union of Crystallography 2013-06-19 /pmc/articles/PMC3770384/ /pubmed/24046669 http://dx.doi.org/10.1107/S1600536813016127 Text en © Al-Suwaidan et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Al-Suwaidan, Ibrahim A.
Abdel-Aziz, Alaa A.-M.
El-Azab, Adel S.
Chidan Kumar, C. S.
Fun, Hoong-Kun
Methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate
title Methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate
title_full Methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate
title_fullStr Methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate
title_full_unstemmed Methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate
title_short Methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate
title_sort methyl 3-[(6-nitro-4-oxo-3-phenyl-3,4-di­hydro­quinazolin-2-yl)sulfan­yl]propano­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3770384/
https://www.ncbi.nlm.nih.gov/pubmed/24046669
http://dx.doi.org/10.1107/S1600536813016127
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