7-Bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5H)-one

In the title compound C(18)H(26)BrNO(2)S, the thia­zepine ring adopts a boat conformation. The dihedral angle between the mean planes through the benzene ring and the four C atoms making up the basal plane of the boat is 35.8 (2)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen b...

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Detalles Bibliográficos
Autores principales: Deepu, C. V., Manjula, M., Pampa, K. J., Bhadregowda, D. G., Lokanath, N. K.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3770397/
https://www.ncbi.nlm.nih.gov/pubmed/24046682
http://dx.doi.org/10.1107/S1600536813013238
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author Deepu, C. V.
Manjula, M.
Pampa, K. J.
Bhadregowda, D. G.
Lokanath, N. K.
author_facet Deepu, C. V.
Manjula, M.
Pampa, K. J.
Bhadregowda, D. G.
Lokanath, N. K.
author_sort Deepu, C. V.
collection PubMed
description In the title compound C(18)H(26)BrNO(2)S, the thia­zepine ring adopts a boat conformation. The dihedral angle between the mean planes through the benzene ring and the four C atoms making up the basal plane of the boat is 35.8 (2)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(8) loops.
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spelling pubmed-37703972013-09-17 7-Bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5H)-one Deepu, C. V. Manjula, M. Pampa, K. J. Bhadregowda, D. G. Lokanath, N. K. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound C(18)H(26)BrNO(2)S, the thia­zepine ring adopts a boat conformation. The dihedral angle between the mean planes through the benzene ring and the four C atoms making up the basal plane of the boat is 35.8 (2)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(8) loops. International Union of Crystallography 2013-06-19 /pmc/articles/PMC3770397/ /pubmed/24046682 http://dx.doi.org/10.1107/S1600536813013238 Text en © Deepu et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Deepu, C. V.
Manjula, M.
Pampa, K. J.
Bhadregowda, D. G.
Lokanath, N. K.
7-Bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5H)-one
title 7-Bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5H)-one
title_full 7-Bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5H)-one
title_fullStr 7-Bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5H)-one
title_full_unstemmed 7-Bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5H)-one
title_short 7-Bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5H)-one
title_sort 7-bromo-3,3-dibutyl-8-meth­oxy-2,3-di­hydro-1,5-benzothia­zepin-4(5h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3770397/
https://www.ncbi.nlm.nih.gov/pubmed/24046682
http://dx.doi.org/10.1107/S1600536813013238
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