1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate

The title compound, C(17)H(18)N(4)O(2)S·CH(3)OH, was synthesized by the condensation reaction of o-meth­oxy­benzaldehyde with thio­carbohydrazide in methanol. The two benzene rings are inclined each to other at 31.7 (1)°. Inter­molecular N—H⋯O and bifurcated O—H⋯N(S) hydrogen bonds link two thio­car...

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Detalles Bibliográficos
Autores principales: Yu, Jianfeng, Tang, Shiming, Zeng, Jingbin, Yan, Zifeng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3770410/
https://www.ncbi.nlm.nih.gov/pubmed/24046695
http://dx.doi.org/10.1107/S1600536813016954
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author Yu, Jianfeng
Tang, Shiming
Zeng, Jingbin
Yan, Zifeng
author_facet Yu, Jianfeng
Tang, Shiming
Zeng, Jingbin
Yan, Zifeng
author_sort Yu, Jianfeng
collection PubMed
description The title compound, C(17)H(18)N(4)O(2)S·CH(3)OH, was synthesized by the condensation reaction of o-meth­oxy­benzaldehyde with thio­carbohydrazide in methanol. The two benzene rings are inclined each to other at 31.7 (1)°. Inter­molecular N—H⋯O and bifurcated O—H⋯N(S) hydrogen bonds link two thio­carbonohydrazide and two solvent mol­ecules into a centrosymmetric unit. These units, related by translation along the b axis, are further aggregated into columns through N—H⋯S hydrogen bonds.
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spelling pubmed-37704102013-09-17 1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate Yu, Jianfeng Tang, Shiming Zeng, Jingbin Yan, Zifeng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(18)N(4)O(2)S·CH(3)OH, was synthesized by the condensation reaction of o-meth­oxy­benzaldehyde with thio­carbohydrazide in methanol. The two benzene rings are inclined each to other at 31.7 (1)°. Inter­molecular N—H⋯O and bifurcated O—H⋯N(S) hydrogen bonds link two thio­carbonohydrazide and two solvent mol­ecules into a centrosymmetric unit. These units, related by translation along the b axis, are further aggregated into columns through N—H⋯S hydrogen bonds. International Union of Crystallography 2013-06-22 /pmc/articles/PMC3770410/ /pubmed/24046695 http://dx.doi.org/10.1107/S1600536813016954 Text en © Yu et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yu, Jianfeng
Tang, Shiming
Zeng, Jingbin
Yan, Zifeng
1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title 1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_full 1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_fullStr 1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_full_unstemmed 1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_short 1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_sort 1,5-bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3770410/
https://www.ncbi.nlm.nih.gov/pubmed/24046695
http://dx.doi.org/10.1107/S1600536813016954
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AT yanzifeng 15bis2methoxybenzylidenethiocarbonohydrazidemethanolmonosolvate

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