Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source

A new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO(4)) nanocrystals with decavanadate (K(6)V(10)O(28) ·9H(2)O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and...

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Detalles Bibliográficos
Autores principales: Li, Quanguo, Zuo, Wenli, Li, Feng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Hindawi Publishing Corporation 2013
Materias:
Research Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3771421/
https://www.ncbi.nlm.nih.gov/pubmed/24068882
http://dx.doi.org/10.1155/2013/127816
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author Li, Quanguo
Zuo, Wenli
Li, Feng
author_facet Li, Quanguo
Zuo, Wenli
Li, Feng
author_sort Li, Quanguo
collection PubMed
description A new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO(4)) nanocrystals with decavanadate (K(6)V(10)O(28) ·9H(2)O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a relatively mild reaction temperature. The EDTA, pH value, and temperature of the reaction systems play important roles in determining the morphologies and growth process of the SmVO(4) products. The products have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), photoluminescence spectra (PL), and UV-Vis spectroscopy.
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spelling pubmed-37714212013-09-25 Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source Li, Quanguo Zuo, Wenli Li, Feng ScientificWorldJournal Research Article A new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO(4)) nanocrystals with decavanadate (K(6)V(10)O(28) ·9H(2)O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a relatively mild reaction temperature. The EDTA, pH value, and temperature of the reaction systems play important roles in determining the morphologies and growth process of the SmVO(4) products. The products have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), photoluminescence spectra (PL), and UV-Vis spectroscopy. Hindawi Publishing Corporation 2013-08-28 /pmc/articles/PMC3771421/ /pubmed/24068882 http://dx.doi.org/10.1155/2013/127816 Text en Copyright © 2013 Quanguo Li et al. https://creativecommons.org/licenses/by/3.0/ This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Research Article
Li, Quanguo
Zuo, Wenli
Li, Feng
Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_full Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_fullStr Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_full_unstemmed Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_short Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_sort chelating ligand-mediated hydrothermal synthesis of samarium orthovanadate with decavanadate as vanadium source
topic Research Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3771421/
https://www.ncbi.nlm.nih.gov/pubmed/24068882
http://dx.doi.org/10.1155/2013/127816
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AT lifeng chelatingligandmediatedhydrothermalsynthesisofsamariumorthovanadatewithdecavanadateasvanadiumsource

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