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2-(Benzylcarbamoyl)nicotinic acid
In the title compound, C(14)H(12)N(2)O(3), the pyridine ring is twisted with respect to the phenyl ring and the carboxylic acid group at angles of 37.1 (5) and 8.1 (3)°, respectively; the phenyl ring forms a dihedral angle of 41.4 (1)° with the mean plane of the C—NH—C=O fragment. An intramolecul...
| Autores principales: | , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2013
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3790388/ https://www.ncbi.nlm.nih.gov/pubmed/24098210 http://dx.doi.org/10.1107/S1600536813024483 |
| _version_ | 1782286586215399424 |
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| author | Mao, Yan-Cao Wu, Hao Shan, Jin-Jun Yan, Ke |
| author_facet | Mao, Yan-Cao Wu, Hao Shan, Jin-Jun Yan, Ke |
| author_sort | Mao, Yan-Cao |
| collection | PubMed |
| description | In the title compound, C(14)H(12)N(2)O(3), the pyridine ring is twisted with respect to the phenyl ring and the carboxylic acid group at angles of 37.1 (5) and 8.1 (3)°, respectively; the phenyl ring forms a dihedral angle of 41.4 (1)° with the mean plane of the C—NH—C=O fragment. An intramolecular O—H⋯O hydrogen bond occurs between the carboxylic acid and carbonyl groups. In the crystal, N—H⋯O hydrogen bonds link molecules into a supramolecular chain running along the a-axis direction. |
| format | Online Article Text |
| id | pubmed-3790388 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2013 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-37903882013-10-04 2-(Benzylcarbamoyl)nicotinic acid Mao, Yan-Cao Wu, Hao Shan, Jin-Jun Yan, Ke Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(12)N(2)O(3), the pyridine ring is twisted with respect to the phenyl ring and the carboxylic acid group at angles of 37.1 (5) and 8.1 (3)°, respectively; the phenyl ring forms a dihedral angle of 41.4 (1)° with the mean plane of the C—NH—C=O fragment. An intramolecular O—H⋯O hydrogen bond occurs between the carboxylic acid and carbonyl groups. In the crystal, N—H⋯O hydrogen bonds link molecules into a supramolecular chain running along the a-axis direction. International Union of Crystallography 2013-09-07 /pmc/articles/PMC3790388/ /pubmed/24098210 http://dx.doi.org/10.1107/S1600536813024483 Text en © Mao et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Mao, Yan-Cao Wu, Hao Shan, Jin-Jun Yan, Ke 2-(Benzylcarbamoyl)nicotinic acid |
| title | 2-(Benzylcarbamoyl)nicotinic acid |
| title_full | 2-(Benzylcarbamoyl)nicotinic acid |
| title_fullStr | 2-(Benzylcarbamoyl)nicotinic acid |
| title_full_unstemmed | 2-(Benzylcarbamoyl)nicotinic acid |
| title_short | 2-(Benzylcarbamoyl)nicotinic acid |
| title_sort | 2-(benzylcarbamoyl)nicotinic acid |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3790388/ https://www.ncbi.nlm.nih.gov/pubmed/24098210 http://dx.doi.org/10.1107/S1600536813024483 |
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