N,N-Diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1H-pyrazol-5-yl]aniline

In the title mol­ecule, C(24)H(26)N(4), the pyrazoline ring assumes an envelope conformation with the aniline-bearing C atom at the flap position. The benzene ring and the pyridine ring form with the pyrazoline ring dihedral angles of 4.53 (1) and 6.26 (1)°, respectively. In turn, the aniline group...

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Detalles Bibliográficos
Autores principales: Zhu, Ying-Zhong, Wang, Hui, Sun, Ping-Ping, Tian, Yu-Peng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3793803/
https://www.ncbi.nlm.nih.gov/pubmed/24109390
http://dx.doi.org/10.1107/S1600536813019879
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author Zhu, Ying-Zhong
Wang, Hui
Sun, Ping-Ping
Tian, Yu-Peng
author_facet Zhu, Ying-Zhong
Wang, Hui
Sun, Ping-Ping
Tian, Yu-Peng
author_sort Zhu, Ying-Zhong
collection PubMed
description In the title mol­ecule, C(24)H(26)N(4), the pyrazoline ring assumes an envelope conformation with the aniline-bearing C atom at the flap position. The benzene ring and the pyridine ring form with the pyrazoline ring dihedral angles of 4.53 (1) and 6.26 (1)°, respectively. In turn, the aniline group is nearly perpendicular to the pyrazoline ring [dihedral angle = 79.96 (1)°]. The ethyl groups of the di­ethyl­amine substituent are disordered over two sets of sites, with an occupancy ratio of 0.624 (8):0.376 (8).
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spelling pubmed-37938032013-10-09 N,N-Diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1H-pyrazol-5-yl]aniline Zhu, Ying-Zhong Wang, Hui Sun, Ping-Ping Tian, Yu-Peng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title mol­ecule, C(24)H(26)N(4), the pyrazoline ring assumes an envelope conformation with the aniline-bearing C atom at the flap position. The benzene ring and the pyridine ring form with the pyrazoline ring dihedral angles of 4.53 (1) and 6.26 (1)°, respectively. In turn, the aniline group is nearly perpendicular to the pyrazoline ring [dihedral angle = 79.96 (1)°]. The ethyl groups of the di­ethyl­amine substituent are disordered over two sets of sites, with an occupancy ratio of 0.624 (8):0.376 (8). International Union of Crystallography 2013-07-27 /pmc/articles/PMC3793803/ /pubmed/24109390 http://dx.doi.org/10.1107/S1600536813019879 Text en © Zhu et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhu, Ying-Zhong
Wang, Hui
Sun, Ping-Ping
Tian, Yu-Peng
N,N-Diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1H-pyrazol-5-yl]aniline
title N,N-Diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1H-pyrazol-5-yl]aniline
title_full N,N-Diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1H-pyrazol-5-yl]aniline
title_fullStr N,N-Diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1H-pyrazol-5-yl]aniline
title_full_unstemmed N,N-Diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1H-pyrazol-5-yl]aniline
title_short N,N-Diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1H-pyrazol-5-yl]aniline
title_sort n,n-diethyl-4-[1-phenyl-3-(pyridin-2-yl)-4,5-di­hydro-1h-pyrazol-5-yl]aniline
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3793803/
https://www.ncbi.nlm.nih.gov/pubmed/24109390
http://dx.doi.org/10.1107/S1600536813019879
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