1,3-Bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate

The asymmetric unit of the title salt, C(16)H(21)N(2)O(2) (+)·PF(6) (−), contains half of the whole ion pair, which has crystallographic mirror symmetry. Two F atoms related by the mirror plane are disordered over two sites of equal occupancy. The dihedral angle between the central ring and the fura...

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Detalles Bibliográficos
Autores principales: Akkurt, Mehmet, Akkoç, Senem, Gök, Yetkin, Tahir, Muhammad Nawaz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3793810/
https://www.ncbi.nlm.nih.gov/pubmed/24109397
http://dx.doi.org/10.1107/S1600536813020187
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author Akkurt, Mehmet
Akkoç, Senem
Gök, Yetkin
Tahir, Muhammad Nawaz
author_facet Akkurt, Mehmet
Akkoç, Senem
Gök, Yetkin
Tahir, Muhammad Nawaz
author_sort Akkurt, Mehmet
collection PubMed
description The asymmetric unit of the title salt, C(16)H(21)N(2)O(2) (+)·PF(6) (−), contains half of the whole ion pair, which has crystallographic mirror symmetry. Two F atoms related by the mirror plane are disordered over two sites of equal occupancy. The dihedral angle between the central ring and the furan ring is 59.3 ()°. In the crystal, the anions and cations are linked through C—H⋯F inter­actions, forming a three-dimensional network.
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spelling pubmed-37938102013-10-09 1,3-Bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate Akkurt, Mehmet Akkoç, Senem Gök, Yetkin Tahir, Muhammad Nawaz Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title salt, C(16)H(21)N(2)O(2) (+)·PF(6) (−), contains half of the whole ion pair, which has crystallographic mirror symmetry. Two F atoms related by the mirror plane are disordered over two sites of equal occupancy. The dihedral angle between the central ring and the furan ring is 59.3 ()°. In the crystal, the anions and cations are linked through C—H⋯F inter­actions, forming a three-dimensional network. International Union of Crystallography 2013-07-27 /pmc/articles/PMC3793810/ /pubmed/24109397 http://dx.doi.org/10.1107/S1600536813020187 Text en © Akkurt et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Akkurt, Mehmet
Akkoç, Senem
Gök, Yetkin
Tahir, Muhammad Nawaz
1,3-Bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate
title 1,3-Bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate
title_full 1,3-Bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate
title_fullStr 1,3-Bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate
title_full_unstemmed 1,3-Bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate
title_short 1,3-Bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate
title_sort 1,3-bis[(5-amino­furan-2-yl)meth­yl]-3,4,5,6-tetra­hydro­pyrimidin-1-ium hexa­fluoro­phosphate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3793810/
https://www.ncbi.nlm.nih.gov/pubmed/24109397
http://dx.doi.org/10.1107/S1600536813020187
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