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Continuous-flow Heck synthesis of 4-methoxybiphenyl and methyl 4-methoxycinnamate in supercritical carbon dioxide expanded solvent solutions

The palladium metal catalysed Heck reaction of 4-iodoanisole with styrene or methyl acrylate has been studied in a continuous plug flow reactor (PFR) using supercritical carbon dioxide (scCO(2)) as the solvent, with THF and methanol as modifiers. The catalyst was 2% palladium on silica and the base...

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Detalles Bibliográficos
Autores principales: Lau, Phei Li, Allen, Ray W K, Styring, Peter
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3869343/
https://www.ncbi.nlm.nih.gov/pubmed/24367454
http://dx.doi.org/10.3762/bjoc.9.325

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