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Synthesis, microstructure, and magnetic properties of monosized Mn( x )Zn( y )Fe(3 − x − y )O(4) ferrite nanocrystals

We report the synthesis and characterization of ferrite nanocrystals which exhibit high crystallinity and narrow size distributions. The three types of samples including Zn ferrite, Mn ferrite, and Mn-Zn ferrite were prepared via a non-aqueous nanoemulsion method. The structural, chemical, and magne...

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Detalles Bibliográficos
Autores principales: Yoon, Hayoung, Lee, Ji Sung, Min, Ji Hyun, Wu, JunHua, Kim, Young Keun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3878439/
https://www.ncbi.nlm.nih.gov/pubmed/24344630
http://dx.doi.org/10.1186/1556-276X-8-530
Descripción
Sumario:We report the synthesis and characterization of ferrite nanocrystals which exhibit high crystallinity and narrow size distributions. The three types of samples including Zn ferrite, Mn ferrite, and Mn-Zn ferrite were prepared via a non-aqueous nanoemulsion method. The structural, chemical, and magnetic properties of the nanocrystals are analyzed by transmission electron microscopy, X-ray diffraction, X-ray fluorescence, and physical property measurement system. The characterization indicates that the three types of ferrite nanocrystals were successfully produced, which show well-behaved magnetic properties, ferrimagnetism at 5 K and superparamagnetism at 300 K, respectively. In addition, the magnetization value of the ferrites increases with the increasing concentration of Mn.