6,7-Diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one

The asymmetric unit of the title compound, C(19)H(19)NOS, contains two independent mol­ecules (A and B), in both of which the 1,3-thia­zepan-4-one ring adopts a chair-type conformation. The dihedral angles between the two phenyl rings are 65.28 (8) and 60.31 (9)° for mol­ecules A and B, respectively...

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Detalles Bibliográficos
Autores principales: Yennawar, Hemant P., Silverberg, Lee J.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3884320/
https://www.ncbi.nlm.nih.gov/pubmed/24454096
http://dx.doi.org/10.1107/S1600536813027979
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author Yennawar, Hemant P.
Silverberg, Lee J.
author_facet Yennawar, Hemant P.
Silverberg, Lee J.
author_sort Yennawar, Hemant P.
collection PubMed
description The asymmetric unit of the title compound, C(19)H(19)NOS, contains two independent mol­ecules (A and B), in both of which the 1,3-thia­zepan-4-one ring adopts a chair-type conformation. The dihedral angles between the two phenyl rings are 65.28 (8) and 60.31 (9)° for mol­ecules A and B, respectively. In the crystal, mol­ecules are linked by weak C—H⋯O inter­actions, resulting in a three-dimensional network.
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spelling pubmed-38843202014-01-17 6,7-Diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one Yennawar, Hemant P. Silverberg, Lee J. Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(19)H(19)NOS, contains two independent mol­ecules (A and B), in both of which the 1,3-thia­zepan-4-one ring adopts a chair-type conformation. The dihedral angles between the two phenyl rings are 65.28 (8) and 60.31 (9)° for mol­ecules A and B, respectively. In the crystal, mol­ecules are linked by weak C—H⋯O inter­actions, resulting in a three-dimensional network. International Union of Crystallography 2013-10-19 /pmc/articles/PMC3884320/ /pubmed/24454096 http://dx.doi.org/10.1107/S1600536813027979 Text en © Yennawar and Silverberg 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yennawar, Hemant P.
Silverberg, Lee J.
6,7-Diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one
title 6,7-Diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one
title_full 6,7-Diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one
title_fullStr 6,7-Diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one
title_full_unstemmed 6,7-Diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one
title_short 6,7-Diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one
title_sort 6,7-diphenyl-5-thia-7-aza­spiro­[2.6]nonan-8-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3884320/
https://www.ncbi.nlm.nih.gov/pubmed/24454096
http://dx.doi.org/10.1107/S1600536813027979
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