4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate

In the title compound, C(15)H(15)NO(4)S, the dihedral angle between the benzene rings is 78.62 (16)°. In the crystal, adjacent mol­ecules are linked along the c axis into C(4) chains through strong N—H⋯O hydrogen bonds. Mol­ecules are further connected through C—H⋯O hydrogen bonds into a hexa­meric...

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Detalles Bibliográficos
Autores principales: Sreenivasa, Swamy, Palakshamurthy, Bandrehalli Siddagangaiah, Tonannavar, Jagdish, Jayashree, Yenagi, Sudha, Achar Gurumurthy, Suchetan, Parameshwar Adimoole
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3884324/
https://www.ncbi.nlm.nih.gov/pubmed/24454100
http://dx.doi.org/10.1107/S1600536813028158
Descripción
Sumario:In the title compound, C(15)H(15)NO(4)S, the dihedral angle between the benzene rings is 78.62 (16)°. In the crystal, adjacent mol­ecules are linked along the c axis into C(4) chains through strong N—H⋯O hydrogen bonds. Mol­ecules are further connected through C—H⋯O hydrogen bonds into a hexa­meric unit generating an R (6) (6)(66) motif. Another C—H⋯O inter­action connects the mol­ecules along the c axis, forming C(5) chains. A region of disordered electron density, most probably disordered methanol–water solvent mol­ecules, was treated with the SQUEEZE routine in PLATON [Spek (2009 ▶). Acta Cryst. D65, 148–155]. The formula mass and unit-cell characteristics do not take into account this disordered solvent.

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