4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate

In the title compound, C(15)H(15)NO(4)S, the dihedral angle between the benzene rings is 78.62 (16)°. In the crystal, adjacent mol­ecules are linked along the c axis into C(4) chains through strong N—H⋯O hydrogen bonds. Mol­ecules are further connected through C—H⋯O hydrogen bonds into a hexa­meric...

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Autores principales: Sreenivasa, Swamy, Palakshamurthy, Bandrehalli Siddagangaiah, Tonannavar, Jagdish, Jayashree, Yenagi, Sudha, Achar Gurumurthy, Suchetan, Parameshwar Adimoole
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3884324/
https://www.ncbi.nlm.nih.gov/pubmed/24454100
http://dx.doi.org/10.1107/S1600536813028158
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author Sreenivasa, Swamy
Palakshamurthy, Bandrehalli Siddagangaiah
Tonannavar, Jagdish
Jayashree, Yenagi
Sudha, Achar Gurumurthy
Suchetan, Parameshwar Adimoole
author_facet Sreenivasa, Swamy
Palakshamurthy, Bandrehalli Siddagangaiah
Tonannavar, Jagdish
Jayashree, Yenagi
Sudha, Achar Gurumurthy
Suchetan, Parameshwar Adimoole
author_sort Sreenivasa, Swamy
collection PubMed
description In the title compound, C(15)H(15)NO(4)S, the dihedral angle between the benzene rings is 78.62 (16)°. In the crystal, adjacent mol­ecules are linked along the c axis into C(4) chains through strong N—H⋯O hydrogen bonds. Mol­ecules are further connected through C—H⋯O hydrogen bonds into a hexa­meric unit generating an R (6) (6)(66) motif. Another C—H⋯O inter­action connects the mol­ecules along the c axis, forming C(5) chains. A region of disordered electron density, most probably disordered methanol–water solvent mol­ecules, was treated with the SQUEEZE routine in PLATON [Spek (2009 ▶). Acta Cryst. D65, 148–155]. The formula mass and unit-cell characteristics do not take into account this disordered solvent.
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spelling pubmed-38843242014-01-17 4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate Sreenivasa, Swamy Palakshamurthy, Bandrehalli Siddagangaiah Tonannavar, Jagdish Jayashree, Yenagi Sudha, Achar Gurumurthy Suchetan, Parameshwar Adimoole Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(15)NO(4)S, the dihedral angle between the benzene rings is 78.62 (16)°. In the crystal, adjacent mol­ecules are linked along the c axis into C(4) chains through strong N—H⋯O hydrogen bonds. Mol­ecules are further connected through C—H⋯O hydrogen bonds into a hexa­meric unit generating an R (6) (6)(66) motif. Another C—H⋯O inter­action connects the mol­ecules along the c axis, forming C(5) chains. A region of disordered electron density, most probably disordered methanol–water solvent mol­ecules, was treated with the SQUEEZE routine in PLATON [Spek (2009 ▶). Acta Cryst. D65, 148–155]. The formula mass and unit-cell characteristics do not take into account this disordered solvent. International Union of Crystallography 2013-10-19 /pmc/articles/PMC3884324/ /pubmed/24454100 http://dx.doi.org/10.1107/S1600536813028158 Text en © Sreenivasa et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Sreenivasa, Swamy
Palakshamurthy, Bandrehalli Siddagangaiah
Tonannavar, Jagdish
Jayashree, Yenagi
Sudha, Achar Gurumurthy
Suchetan, Parameshwar Adimoole
4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate
title 4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate
title_full 4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate
title_fullStr 4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate
title_full_unstemmed 4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate
title_short 4-Meth­oxy-N-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate
title_sort 4-meth­oxy-n-[(4-methyl­phen­yl)sulfon­yl]benzamide including an unknown solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3884324/
https://www.ncbi.nlm.nih.gov/pubmed/24454100
http://dx.doi.org/10.1107/S1600536813028158
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