Cargando…
8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate
In the crystal structure of the title salt hydrate, C(9)H(8)NO(+)·HSO(4) (−)·H(2)O, the quinoline N—H atoms are hydrogen bonded to the bisulfate anions. The bisulfate anions and water molecules are linked together by O—H⋯O hydrogen-bonding interactions. The cations and anions form separate layer...
Autores principales: | , , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2013
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3884397/ https://www.ncbi.nlm.nih.gov/pubmed/24427083 http://dx.doi.org/10.1107/S1600536813022319 |
_version_ | 1782298581274722304 |
---|---|
author | Damous, Maamar Dénès, George Bouacida, Sofiane Hamlaoui, Meriem Merazig, Hocine Daran, Jean-Claude |
author_facet | Damous, Maamar Dénès, George Bouacida, Sofiane Hamlaoui, Meriem Merazig, Hocine Daran, Jean-Claude |
author_sort | Damous, Maamar |
collection | PubMed |
description | In the crystal structure of the title salt hydrate, C(9)H(8)NO(+)·HSO(4) (−)·H(2)O, the quinoline N—H atoms are hydrogen bonded to the bisulfate anions. The bisulfate anions and water molecules are linked together by O—H⋯O hydrogen-bonding interactions. The cations and anions form separate layers alternating along the c axis, which are linked by N—H⋯O and O—H⋯O hydrogen bonds into a two-dimensional network parallel to (100). Further O—H⋯O contacts connect these layers, forming a three-dimensional network, in which two R (4) (4)(12) rings and C (2) (2)(13) infinite chains can be identified. |
format | Online Article Text |
id | pubmed-3884397 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2013 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-38843972014-01-14 8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate Damous, Maamar Dénès, George Bouacida, Sofiane Hamlaoui, Meriem Merazig, Hocine Daran, Jean-Claude Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title salt hydrate, C(9)H(8)NO(+)·HSO(4) (−)·H(2)O, the quinoline N—H atoms are hydrogen bonded to the bisulfate anions. The bisulfate anions and water molecules are linked together by O—H⋯O hydrogen-bonding interactions. The cations and anions form separate layers alternating along the c axis, which are linked by N—H⋯O and O—H⋯O hydrogen bonds into a two-dimensional network parallel to (100). Further O—H⋯O contacts connect these layers, forming a three-dimensional network, in which two R (4) (4)(12) rings and C (2) (2)(13) infinite chains can be identified. International Union of Crystallography 2013-08-21 /pmc/articles/PMC3884397/ /pubmed/24427083 http://dx.doi.org/10.1107/S1600536813022319 Text en © Damous et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Damous, Maamar Dénès, George Bouacida, Sofiane Hamlaoui, Meriem Merazig, Hocine Daran, Jean-Claude 8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate |
title | 8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate |
title_full | 8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate |
title_fullStr | 8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate |
title_full_unstemmed | 8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate |
title_short | 8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate |
title_sort | 8-hydroxyquinolin-1-ium hydrogen sulfate monohydrate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3884397/ https://www.ncbi.nlm.nih.gov/pubmed/24427083 http://dx.doi.org/10.1107/S1600536813022319 |
work_keys_str_mv | AT damousmaamar 8hydroxyquinolin1iumhydrogensulfatemonohydrate AT denesgeorge 8hydroxyquinolin1iumhydrogensulfatemonohydrate AT bouacidasofiane 8hydroxyquinolin1iumhydrogensulfatemonohydrate AT hamlaouimeriem 8hydroxyquinolin1iumhydrogensulfatemonohydrate AT merazighocine 8hydroxyquinolin1iumhydrogensulfatemonohydrate AT daranjeanclaude 8hydroxyquinolin1iumhydrogensulfatemonohydrate |