Cargando…
4-Amino-12-methylsulfonyloxy-[2.2]paracyclophane
The title compound, C(17)H(19)NO(3)S, was synthesized from 4-benzhydrylideneamino-12-hydroxy-[2.2]paracyclophane and methanesulfonyl chloride. In the molecule, the distance between the centroids of two aromatic rings is 2.960 (5) Å. In the crystal, weak N—H⋯O and C—H⋯O hydrogen bonds link the...
Autores principales: | , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2013
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3914068/ https://www.ncbi.nlm.nih.gov/pubmed/24526969 http://dx.doi.org/10.1107/S1600536813032595 |
_version_ | 1782302337580138496 |
---|---|
author | Meng, Xiangchao Duan, Wenzeng Han, Yinfeng |
author_facet | Meng, Xiangchao Duan, Wenzeng Han, Yinfeng |
author_sort | Meng, Xiangchao |
collection | PubMed |
description | The title compound, C(17)H(19)NO(3)S, was synthesized from 4-benzhydrylideneamino-12-hydroxy-[2.2]paracyclophane and methanesulfonyl chloride. In the molecule, the distance between the centroids of two aromatic rings is 2.960 (5) Å. In the crystal, weak N—H⋯O and C—H⋯O hydrogen bonds link the molecules into layers parallel to the ac plane. |
format | Online Article Text |
id | pubmed-3914068 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2013 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-39140682014-02-13 4-Amino-12-methylsulfonyloxy-[2.2]paracyclophane Meng, Xiangchao Duan, Wenzeng Han, Yinfeng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(19)NO(3)S, was synthesized from 4-benzhydrylideneamino-12-hydroxy-[2.2]paracyclophane and methanesulfonyl chloride. In the molecule, the distance between the centroids of two aromatic rings is 2.960 (5) Å. In the crystal, weak N—H⋯O and C—H⋯O hydrogen bonds link the molecules into layers parallel to the ac plane. International Union of Crystallography 2013-12-07 /pmc/articles/PMC3914068/ /pubmed/24526969 http://dx.doi.org/10.1107/S1600536813032595 Text en © Meng et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Meng, Xiangchao Duan, Wenzeng Han, Yinfeng 4-Amino-12-methylsulfonyloxy-[2.2]paracyclophane |
title | 4-Amino-12-methylsulfonyloxy-[2.2]paracyclophane |
title_full | 4-Amino-12-methylsulfonyloxy-[2.2]paracyclophane |
title_fullStr | 4-Amino-12-methylsulfonyloxy-[2.2]paracyclophane |
title_full_unstemmed | 4-Amino-12-methylsulfonyloxy-[2.2]paracyclophane |
title_short | 4-Amino-12-methylsulfonyloxy-[2.2]paracyclophane |
title_sort | 4-amino-12-methylsulfonyloxy-[2.2]paracyclophane |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3914068/ https://www.ncbi.nlm.nih.gov/pubmed/24526969 http://dx.doi.org/10.1107/S1600536813032595 |
work_keys_str_mv | AT mengxiangchao 4amino12methylsulfonyloxy22paracyclophane AT duanwenzeng 4amino12methylsulfonyloxy22paracyclophane AT hanyinfeng 4amino12methylsulfonyloxy22paracyclophane |