N,N-Dimethyl-3-phenyl­isoxazole-5-carbox­amide

In the title compound, C(12)H(12)N(2)O(2), synthesized by ammonolysis of 3-phenyl­isoxazole-5-carbonyl chloride in di­chloro­methane, the dihedral angle between the isoxazole ring and the phenyl ring is 14.05 (7)°. In the crystal, centrosym­metrically related mol­ecules are linked into dimers by pai...

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Detalles Bibliográficos
Autores principales: Wang, Li, Li, Ya-Jun, Li, Zheng-Wei, Liu, Kai-Ge, Zhang, Shao-Hua
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3914115/
https://www.ncbi.nlm.nih.gov/pubmed/24527022
http://dx.doi.org/10.1107/S1600536813033199
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author Wang, Li
Li, Ya-Jun
Li, Zheng-Wei
Liu, Kai-Ge
Zhang, Shao-Hua
author_facet Wang, Li
Li, Ya-Jun
Li, Zheng-Wei
Liu, Kai-Ge
Zhang, Shao-Hua
author_sort Wang, Li
collection PubMed
description In the title compound, C(12)H(12)N(2)O(2), synthesized by ammonolysis of 3-phenyl­isoxazole-5-carbonyl chloride in di­chloro­methane, the dihedral angle between the isoxazole ring and the phenyl ring is 14.05 (7)°. In the crystal, centrosym­metrically related mol­ecules are linked into dimers by pairs of C—H⋯O hydrogen bonds, generating rings of graph-set motif R (2) (2)(10).
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spelling pubmed-39141152014-02-13 N,N-Dimethyl-3-phenyl­isoxazole-5-carbox­amide Wang, Li Li, Ya-Jun Li, Zheng-Wei Liu, Kai-Ge Zhang, Shao-Hua Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(12)H(12)N(2)O(2), synthesized by ammonolysis of 3-phenyl­isoxazole-5-carbonyl chloride in di­chloro­methane, the dihedral angle between the isoxazole ring and the phenyl ring is 14.05 (7)°. In the crystal, centrosym­metrically related mol­ecules are linked into dimers by pairs of C—H⋯O hydrogen bonds, generating rings of graph-set motif R (2) (2)(10). International Union of Crystallography 2013-12-24 /pmc/articles/PMC3914115/ /pubmed/24527022 http://dx.doi.org/10.1107/S1600536813033199 Text en © Wang et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Li
Li, Ya-Jun
Li, Zheng-Wei
Liu, Kai-Ge
Zhang, Shao-Hua
N,N-Dimethyl-3-phenyl­isoxazole-5-carbox­amide
title N,N-Dimethyl-3-phenyl­isoxazole-5-carbox­amide
title_full N,N-Dimethyl-3-phenyl­isoxazole-5-carbox­amide
title_fullStr N,N-Dimethyl-3-phenyl­isoxazole-5-carbox­amide
title_full_unstemmed N,N-Dimethyl-3-phenyl­isoxazole-5-carbox­amide
title_short N,N-Dimethyl-3-phenyl­isoxazole-5-carbox­amide
title_sort n,n-dimethyl-3-phenyl­isoxazole-5-carbox­amide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3914115/
https://www.ncbi.nlm.nih.gov/pubmed/24527022
http://dx.doi.org/10.1107/S1600536813033199
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