Phase Transformation of VO(2) Nanoparticles Assisted by Microwave Heating

The microwave assisted synthesis nowadays attracts a great deal of attention. Monoclinic phase VO(2) (M) was prepared from NH(4)VO(3) and H(2)C(2)O(4) · 2H(2)O by a rapid microwave assisted technique. The synthesis parameters, microwave irradiation time, microwave power, and calcinations temperature...

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Detalles Bibliográficos
Autores principales: Phoempoon, Phatcharee, Sikong, Lek.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Hindawi Publishing Corporation 2014
Materias:
Research Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3932267/
https://www.ncbi.nlm.nih.gov/pubmed/24688438
http://dx.doi.org/10.1155/2014/841418
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author Phoempoon, Phatcharee
Sikong, Lek.
author_facet Phoempoon, Phatcharee
Sikong, Lek.
author_sort Phoempoon, Phatcharee
collection PubMed
description The microwave assisted synthesis nowadays attracts a great deal of attention. Monoclinic phase VO(2) (M) was prepared from NH(4)VO(3) and H(2)C(2)O(4) · 2H(2)O by a rapid microwave assisted technique. The synthesis parameters, microwave irradiation time, microwave power, and calcinations temperature were systematically varied and their influences on the structure and morphology were evaluated. The microwave power level has been carried out in range 180–600 W. TEM analysis demonstrated nanosized samples. The structural and morphological properties were measured using XRD, TEM, and thermal analyses. The variations of vanadium phase led to thermochromic properties.
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spelling pubmed-39322672014-03-31 Phase Transformation of VO(2) Nanoparticles Assisted by Microwave Heating Phoempoon, Phatcharee Sikong, Lek. ScientificWorldJournal Research Article The microwave assisted synthesis nowadays attracts a great deal of attention. Monoclinic phase VO(2) (M) was prepared from NH(4)VO(3) and H(2)C(2)O(4) · 2H(2)O by a rapid microwave assisted technique. The synthesis parameters, microwave irradiation time, microwave power, and calcinations temperature were systematically varied and their influences on the structure and morphology were evaluated. The microwave power level has been carried out in range 180–600 W. TEM analysis demonstrated nanosized samples. The structural and morphological properties were measured using XRD, TEM, and thermal analyses. The variations of vanadium phase led to thermochromic properties. Hindawi Publishing Corporation 2014-02-04 /pmc/articles/PMC3932267/ /pubmed/24688438 http://dx.doi.org/10.1155/2014/841418 Text en Copyright © 2014 P. Phoempoon and L. Sikong. https://creativecommons.org/licenses/by/3.0/ This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Research Article
Phoempoon, Phatcharee
Sikong, Lek.
Phase Transformation of VO(2) Nanoparticles Assisted by Microwave Heating
title Phase Transformation of VO(2) Nanoparticles Assisted by Microwave Heating
title_full Phase Transformation of VO(2) Nanoparticles Assisted by Microwave Heating
title_fullStr Phase Transformation of VO(2) Nanoparticles Assisted by Microwave Heating
title_full_unstemmed Phase Transformation of VO(2) Nanoparticles Assisted by Microwave Heating
title_short Phase Transformation of VO(2) Nanoparticles Assisted by Microwave Heating
title_sort phase transformation of vo(2) nanoparticles assisted by microwave heating
topic Research Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3932267/
https://www.ncbi.nlm.nih.gov/pubmed/24688438
http://dx.doi.org/10.1155/2014/841418
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