Cargando…
SAXS investigation of nanoporous structure of thermal-modified carbon materials
The article investigates the effect of thermal modification of porous carbon material (PCM), obtained from plant feedstock, on its morphology and fractal structure by small-angle X-ray scattering (SAXS) method. The analysis of the scattering intensity curves serve the basis for calculating the param...
Autores principales: | , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Springer
2014
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3985573/ https://www.ncbi.nlm.nih.gov/pubmed/24708842 http://dx.doi.org/10.1186/1556-276X-9-160 |
_version_ | 1782311589460836352 |
---|---|
author | Ostafiychuk, Bogdan K Mandzyuk, Volodymyr I Kulyk, Yuriy O Nagirna, Nadiia I |
author_facet | Ostafiychuk, Bogdan K Mandzyuk, Volodymyr I Kulyk, Yuriy O Nagirna, Nadiia I |
author_sort | Ostafiychuk, Bogdan K |
collection | PubMed |
description | The article investigates the effect of thermal modification of porous carbon material (PCM), obtained from plant feedstock, on its morphology and fractal structure by small-angle X-ray scattering (SAXS) method. The analysis of the scattering intensity curves serve the basis for calculating the parameters of the PCM porous structure: the Porod constant, the Porod invariant, average pore radius, specific surface area, and mass and surface fractal dimensions. It has been found out that the PCMs obtained have fractal structure, formed from mass and surface fractals, the sizes of which increase at the growth of temperature and modification time. PACS: 81.05.Uw; 61.05.cf; 82.47.Aa |
format | Online Article Text |
id | pubmed-3985573 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2014 |
publisher | Springer |
record_format | MEDLINE/PubMed |
spelling | pubmed-39855732014-04-17 SAXS investigation of nanoporous structure of thermal-modified carbon materials Ostafiychuk, Bogdan K Mandzyuk, Volodymyr I Kulyk, Yuriy O Nagirna, Nadiia I Nanoscale Res Lett Nano Express The article investigates the effect of thermal modification of porous carbon material (PCM), obtained from plant feedstock, on its morphology and fractal structure by small-angle X-ray scattering (SAXS) method. The analysis of the scattering intensity curves serve the basis for calculating the parameters of the PCM porous structure: the Porod constant, the Porod invariant, average pore radius, specific surface area, and mass and surface fractal dimensions. It has been found out that the PCMs obtained have fractal structure, formed from mass and surface fractals, the sizes of which increase at the growth of temperature and modification time. PACS: 81.05.Uw; 61.05.cf; 82.47.Aa Springer 2014-04-03 /pmc/articles/PMC3985573/ /pubmed/24708842 http://dx.doi.org/10.1186/1556-276X-9-160 Text en Copyright © 2014 Ostafiychuk et al.; licensee Springer. http://creativecommons.org/licenses/by/2.0 This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly credited. |
spellingShingle | Nano Express Ostafiychuk, Bogdan K Mandzyuk, Volodymyr I Kulyk, Yuriy O Nagirna, Nadiia I SAXS investigation of nanoporous structure of thermal-modified carbon materials |
title | SAXS investigation of nanoporous structure of thermal-modified carbon materials |
title_full | SAXS investigation of nanoporous structure of thermal-modified carbon materials |
title_fullStr | SAXS investigation of nanoporous structure of thermal-modified carbon materials |
title_full_unstemmed | SAXS investigation of nanoporous structure of thermal-modified carbon materials |
title_short | SAXS investigation of nanoporous structure of thermal-modified carbon materials |
title_sort | saxs investigation of nanoporous structure of thermal-modified carbon materials |
topic | Nano Express |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3985573/ https://www.ncbi.nlm.nih.gov/pubmed/24708842 http://dx.doi.org/10.1186/1556-276X-9-160 |
work_keys_str_mv | AT ostafiychukbogdank saxsinvestigationofnanoporousstructureofthermalmodifiedcarbonmaterials AT mandzyukvolodymyri saxsinvestigationofnanoporousstructureofthermalmodifiedcarbonmaterials AT kulykyuriyo saxsinvestigationofnanoporousstructureofthermalmodifiedcarbonmaterials AT nagirnanadiiai saxsinvestigationofnanoporousstructureofthermalmodifiedcarbonmaterials |