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1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea
In the title compound, C(14)H(11)Cl(2)N(5)O, the plane of the 1H-imidazo[4,5-c]pyridine ring system [r.m.s. deviation = 0.087 (19) Å] makes a dihedral angle of 4.87 (10)° with the terminal phenyl ring. An intramolecular N—H⋯N hydrogen bond stabilizes the molecular conformation. In the crystal, N—H...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2014
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998316/ https://www.ncbi.nlm.nih.gov/pubmed/24764877 http://dx.doi.org/10.1107/S1600536814000695 |
| _version_ | 1782313335616700416 |
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| author | Devaru, Venkatesh B. Vinduvahini, M. Madaiah, M. Revanasiddappa, H. D. Devarajegowda, H. C. |
| author_facet | Devaru, Venkatesh B. Vinduvahini, M. Madaiah, M. Revanasiddappa, H. D. Devarajegowda, H. C. |
| author_sort | Devaru, Venkatesh B. |
| collection | PubMed |
| description | In the title compound, C(14)H(11)Cl(2)N(5)O, the plane of the 1H-imidazo[4,5-c]pyridine ring system [r.m.s. deviation = 0.087 (19) Å] makes a dihedral angle of 4.87 (10)° with the terminal phenyl ring. An intramolecular N—H⋯N hydrogen bond stabilizes the molecular conformation. In the crystal, N—H⋯O hydrogen bonds link the molecules into inversion dimers. These dimers are connected by π–π interactions between imidazole rings [shortest centroid–centroid distance = 3.4443 (14) Å]. |
| format | Online Article Text |
| id | pubmed-3998316 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2014 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-39983162014-04-24 1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea Devaru, Venkatesh B. Vinduvahini, M. Madaiah, M. Revanasiddappa, H. D. Devarajegowda, H. C. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(11)Cl(2)N(5)O, the plane of the 1H-imidazo[4,5-c]pyridine ring system [r.m.s. deviation = 0.087 (19) Å] makes a dihedral angle of 4.87 (10)° with the terminal phenyl ring. An intramolecular N—H⋯N hydrogen bond stabilizes the molecular conformation. In the crystal, N—H⋯O hydrogen bonds link the molecules into inversion dimers. These dimers are connected by π–π interactions between imidazole rings [shortest centroid–centroid distance = 3.4443 (14) Å]. International Union of Crystallography 2014-01-18 /pmc/articles/PMC3998316/ /pubmed/24764877 http://dx.doi.org/10.1107/S1600536814000695 Text en © Devaru et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Devaru, Venkatesh B. Vinduvahini, M. Madaiah, M. Revanasiddappa, H. D. Devarajegowda, H. C. 1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea |
| title | 1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea |
| title_full | 1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea |
| title_fullStr | 1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea |
| title_full_unstemmed | 1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea |
| title_short | 1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea |
| title_sort | 1-(6-chloro-1-methyl-1h-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998316/ https://www.ncbi.nlm.nih.gov/pubmed/24764877 http://dx.doi.org/10.1107/S1600536814000695 |
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