N-Phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide

The conformation of the title mol­ecule, C(17)H(17)N(3)S, is stabilized by an intra­molecular N—H⋯N hydrogen bond involving the azometinic group. The dihedral angle between the two aromatic rings is 36.49 (06)°. The non-aromatic ring of the tetra­lone substituent adopts a sofa conformation. In the c...

Descripción completa

Detalles Bibliográficos
Autores principales: de Oliveira, Adriano Bof, Feitosa, Bárbara Regina Santos, Näther, Christian, Jess, Inke
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998352/
https://www.ncbi.nlm.nih.gov/pubmed/24764913
http://dx.doi.org/10.1107/S1600536814001585
_version_ 1782313343784058880
author de Oliveira, Adriano Bof
Feitosa, Bárbara Regina Santos
Näther, Christian
Jess, Inke
author_facet de Oliveira, Adriano Bof
Feitosa, Bárbara Regina Santos
Näther, Christian
Jess, Inke
author_sort de Oliveira, Adriano Bof
collection PubMed
description The conformation of the title mol­ecule, C(17)H(17)N(3)S, is stabilized by an intra­molecular N—H⋯N hydrogen bond involving the azometinic group. The dihedral angle between the two aromatic rings is 36.49 (06)°. The non-aromatic ring of the tetra­lone substituent adopts a sofa conformation. In the crystal, mol­ecules are linked by pairs of N—H⋯S hydrogen bonds related via centres of symmetry, forming dimers.
format Online
Article
Text
id pubmed-3998352
institution National Center for Biotechnology Information
language English
publishDate 2014
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-39983522014-04-24 N-Phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide de Oliveira, Adriano Bof Feitosa, Bárbara Regina Santos Näther, Christian Jess, Inke Acta Crystallogr Sect E Struct Rep Online Organic Papers The conformation of the title mol­ecule, C(17)H(17)N(3)S, is stabilized by an intra­molecular N—H⋯N hydrogen bond involving the azometinic group. The dihedral angle between the two aromatic rings is 36.49 (06)°. The non-aromatic ring of the tetra­lone substituent adopts a sofa conformation. In the crystal, mol­ecules are linked by pairs of N—H⋯S hydrogen bonds related via centres of symmetry, forming dimers. International Union of Crystallography 2014-01-25 /pmc/articles/PMC3998352/ /pubmed/24764913 http://dx.doi.org/10.1107/S1600536814001585 Text en © Oliveira et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
de Oliveira, Adriano Bof
Feitosa, Bárbara Regina Santos
Näther, Christian
Jess, Inke
N-Phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide
title N-Phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide
title_full N-Phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide
title_fullStr N-Phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide
title_full_unstemmed N-Phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide
title_short N-Phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide
title_sort n-phenyl-2-(1,2,3,4-tetra­hydro­naph­thalen-1-yl­idene)hydrazinecarbo­thio­amide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998352/
https://www.ncbi.nlm.nih.gov/pubmed/24764913
http://dx.doi.org/10.1107/S1600536814001585
work_keys_str_mv AT deoliveiraadrianobof nphenyl21234tetrahydronaphthalen1ylidenehydrazinecarbothioamide
AT feitosabarbarareginasantos nphenyl21234tetrahydronaphthalen1ylidenehydrazinecarbothioamide
AT natherchristian nphenyl21234tetrahydronaphthalen1ylidenehydrazinecarbothioamide
AT jessinke nphenyl21234tetrahydronaphthalen1ylidenehydrazinecarbothioamide

Ejemplares similares