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[2-(3,4-Di­meth­oxy­phen­yl)eth­yl](3-{N-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate

The asymmetric unit of the title hydrated salt, C(24)H(35)N(2)O(5) (+)·Cl(−)·2H(2)O, contains one organic cation that has its protonation site at the amine function, one chloride anion and two lattice water mol­ecules. In the crystal, one pair of lattice water mol­ecules and two chloride anions form...

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Detalles Bibliográficos
Autores principales: Saidov, Abdusalom Sh., Turgunov, Kambarali K.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998369/
https://www.ncbi.nlm.nih.gov/pubmed/24764930
http://dx.doi.org/10.1107/S1600536814001998
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author Saidov, Abdusalom Sh.
Turgunov, Kambarali K.
author_facet Saidov, Abdusalom Sh.
Turgunov, Kambarali K.
author_sort Saidov, Abdusalom Sh.
collection PubMed
description The asymmetric unit of the title hydrated salt, C(24)H(35)N(2)O(5) (+)·Cl(−)·2H(2)O, contains one organic cation that has its protonation site at the amine function, one chloride anion and two lattice water mol­ecules. In the crystal, one pair of lattice water mol­ecules and two chloride anions form a four-membered centrosymmetric hydrogen-bond cycle. In addition, O—H⋯O, N—H⋯O and N—H⋯Cl hydrogen bonds involving the N—H groups, the water mol­ecules and the C=O group are observed. As a result, a hydrogen-bonded layer parallel to (100) is formed. The thickness of such a layer corresponds to the length of the a axis [21.977 (3) Å].
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spelling pubmed-39983692014-04-24 [2-(3,4-Di­meth­oxy­phen­yl)eth­yl](3-{N-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate Saidov, Abdusalom Sh. Turgunov, Kambarali K. Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title hydrated salt, C(24)H(35)N(2)O(5) (+)·Cl(−)·2H(2)O, contains one organic cation that has its protonation site at the amine function, one chloride anion and two lattice water mol­ecules. In the crystal, one pair of lattice water mol­ecules and two chloride anions form a four-membered centrosymmetric hydrogen-bond cycle. In addition, O—H⋯O, N—H⋯O and N—H⋯Cl hydrogen bonds involving the N—H groups, the water mol­ecules and the C=O group are observed. As a result, a hydrogen-bonded layer parallel to (100) is formed. The thickness of such a layer corresponds to the length of the a axis [21.977 (3) Å]. International Union of Crystallography 2014-01-31 /pmc/articles/PMC3998369/ /pubmed/24764930 http://dx.doi.org/10.1107/S1600536814001998 Text en © Saidov and Turgunov 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saidov, Abdusalom Sh.
Turgunov, Kambarali K.
[2-(3,4-Di­meth­oxy­phen­yl)eth­yl](3-{N-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate
title [2-(3,4-Di­meth­oxy­phen­yl)eth­yl](3-{N-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate
title_full [2-(3,4-Di­meth­oxy­phen­yl)eth­yl](3-{N-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate
title_fullStr [2-(3,4-Di­meth­oxy­phen­yl)eth­yl](3-{N-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate
title_full_unstemmed [2-(3,4-Di­meth­oxy­phen­yl)eth­yl](3-{N-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate
title_short [2-(3,4-Di­meth­oxy­phen­yl)eth­yl](3-{N-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate
title_sort [2-(3,4-di­meth­oxy­phen­yl)eth­yl](3-{n-[2-(3,4-di­meth­oxy­phen­yl)eth­yl]carbamo­yl}prop­yl)aza­nium chloride dihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998369/
https://www.ncbi.nlm.nih.gov/pubmed/24764930
http://dx.doi.org/10.1107/S1600536814001998
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AT turgunovkambaralik 234dimethoxyphenylethyl3n234dimethoxyphenylethylcarbamoylpropylazaniumchloridedihydrate