5-Phenyl-1,2,5-di­thia­zepane

In the title compound, C(10)H(13)NS(2), the seven-membered ring adopts a chair conformation. The S—S bond length is 2.0406 (5) Å and the C—S—S—C torsion angle is −83.89 (7)°. The amine group is sp (2)-hybridized. In the crystal, mol­ecules are linked into chains along [001] by weak inter­molecular S...

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Autores principales: Mitchell, Lauren A., Mejía, Michelle L., Keskin, Seyma Gören, Holliday, Bradley J.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998476/
https://www.ncbi.nlm.nih.gov/pubmed/24764994
http://dx.doi.org/10.1107/S1600536814002207
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author Mitchell, Lauren A.
Mejía, Michelle L.
Keskin, Seyma Gören
Holliday, Bradley J.
author_facet Mitchell, Lauren A.
Mejía, Michelle L.
Keskin, Seyma Gören
Holliday, Bradley J.
author_sort Mitchell, Lauren A.
collection PubMed
description In the title compound, C(10)H(13)NS(2), the seven-membered ring adopts a chair conformation. The S—S bond length is 2.0406 (5) Å and the C—S—S—C torsion angle is −83.89 (7)°. The amine group is sp (2)-hybridized. In the crystal, mol­ecules are linked into chains along [001] by weak inter­molecular S⋯S contacts of 3.5246 (5) Å.
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spelling pubmed-39984762014-04-24 5-Phenyl-1,2,5-di­thia­zepane Mitchell, Lauren A. Mejía, Michelle L. Keskin, Seyma Gören Holliday, Bradley J. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(13)NS(2), the seven-membered ring adopts a chair conformation. The S—S bond length is 2.0406 (5) Å and the C—S—S—C torsion angle is −83.89 (7)°. The amine group is sp (2)-hybridized. In the crystal, mol­ecules are linked into chains along [001] by weak inter­molecular S⋯S contacts of 3.5246 (5) Å. International Union of Crystallography 2014-02-12 /pmc/articles/PMC3998476/ /pubmed/24764994 http://dx.doi.org/10.1107/S1600536814002207 Text en © Mitchell et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mitchell, Lauren A.
Mejía, Michelle L.
Keskin, Seyma Gören
Holliday, Bradley J.
5-Phenyl-1,2,5-di­thia­zepane
title 5-Phenyl-1,2,5-di­thia­zepane
title_full 5-Phenyl-1,2,5-di­thia­zepane
title_fullStr 5-Phenyl-1,2,5-di­thia­zepane
title_full_unstemmed 5-Phenyl-1,2,5-di­thia­zepane
title_short 5-Phenyl-1,2,5-di­thia­zepane
title_sort 5-phenyl-1,2,5-di­thia­zepane
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998476/
https://www.ncbi.nlm.nih.gov/pubmed/24764994
http://dx.doi.org/10.1107/S1600536814002207
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