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2-Cyclo­heptyl­idene-N-phenyl­hydrazine­carbo­thio­amide

In the title compound, C(14)H(19)N(3)S, the seven-membered cyclo­heptane ring adopts a chair conformation. An intra­molecular N—H⋯N hydrogen bond [graph-set motif S(5)] is present in the N—N—C—N chain between the ring systems. An intra­molecular C—H⋯S contact also occurs. In the crystal, pairs of mo...

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Detalles Bibliográficos
Autores principales: Akkurt, Mehmet, Mohamed, Shaaban K., Mague, Joel T., Hassan, Alaa A., Albayati, Mustafa R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998488/
https://www.ncbi.nlm.nih.gov/pubmed/24765045
http://dx.doi.org/10.1107/S1600536814003948
Descripción
Sumario:In the title compound, C(14)H(19)N(3)S, the seven-membered cyclo­heptane ring adopts a chair conformation. An intra­molecular N—H⋯N hydrogen bond [graph-set motif S(5)] is present in the N—N—C—N chain between the ring systems. An intra­molecular C—H⋯S contact also occurs. In the crystal, pairs of mol­ecules form centrosymmetric dimers through N—H⋯S hydrogen bonds [graph-set R (2) (2)(8)]. These dimers are connected by C—H⋯S inter­actions with an R (2) (2)(14) motif.