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N-(12-Amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide

The title compound, C(23)H(22)N(2)O(2)S, crystallizes with the 4-methyl­benzene­sulfonamide entity oriented towards the center of the bridgehead C atoms with a C—N—S—C torsion angle of −61.3 (2)°. The mol­ecule features an intra­molecular N—H⋯N hydrogen bond. Weak C—H⋯O and C—H⋯π inter­actions aid i...

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Detalles Bibliográficos
Autores principales: Mague, Joel T., Abdel-Aziz, Alaa A.-M., El-Azab, Adel S., El-Sherbeny, Magda A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998504/
https://www.ncbi.nlm.nih.gov/pubmed/24764968
http://dx.doi.org/10.1107/S1600536814002189
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author Mague, Joel T.
Abdel-Aziz, Alaa A.-M.
El-Azab, Adel S.
El-Sherbeny, Magda A.
author_facet Mague, Joel T.
Abdel-Aziz, Alaa A.-M.
El-Azab, Adel S.
El-Sherbeny, Magda A.
author_sort Mague, Joel T.
collection PubMed
description The title compound, C(23)H(22)N(2)O(2)S, crystallizes with the 4-methyl­benzene­sulfonamide entity oriented towards the center of the bridgehead C atoms with a C—N—S—C torsion angle of −61.3 (2)°. The mol­ecule features an intra­molecular N—H⋯N hydrogen bond. Weak C—H⋯O and C—H⋯π inter­actions aid in forming the three-dimensional supra­molecular structure.
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spelling pubmed-39985042014-04-24 N-(12-Amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide Mague, Joel T. Abdel-Aziz, Alaa A.-M. El-Azab, Adel S. El-Sherbeny, Magda A. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(23)H(22)N(2)O(2)S, crystallizes with the 4-methyl­benzene­sulfonamide entity oriented towards the center of the bridgehead C atoms with a C—N—S—C torsion angle of −61.3 (2)°. The mol­ecule features an intra­molecular N—H⋯N hydrogen bond. Weak C—H⋯O and C—H⋯π inter­actions aid in forming the three-dimensional supra­molecular structure. International Union of Crystallography 2014-02-05 /pmc/articles/PMC3998504/ /pubmed/24764968 http://dx.doi.org/10.1107/S1600536814002189 Text en © Mague et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mague, Joel T.
Abdel-Aziz, Alaa A.-M.
El-Azab, Adel S.
El-Sherbeny, Magda A.
N-(12-Amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide
title N-(12-Amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide
title_full N-(12-Amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide
title_fullStr N-(12-Amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide
title_full_unstemmed N-(12-Amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide
title_short N-(12-Amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide
title_sort n-(12-amino-9,10-di­hydro-9,10-ethano­anthracen-11-yl)-4-methyl­benzene­sulfonamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998504/
https://www.ncbi.nlm.nih.gov/pubmed/24764968
http://dx.doi.org/10.1107/S1600536814002189
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