4-Nitro­phthalamide

In the title compound, C(8)H(7)N(3)O(4) (systematic name: 4-nitro­benzene-1,2-dicarboxamide), each of the substituents is twisted out of the plane of the benzene ring to which it is attached [dihedral angles of 11.36 (2)° for the nitro group, and 60.89 (6) and 34.39 (6)° for the amide groups]. The a...

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Autores principales: Jan, Chin Yee, Shamsudin, Norzianah Binti Haji, Tan, Ai Ling, Young, David J., Ng, Seik Weng, Tiekink, Edward R. T.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998509/
https://www.ncbi.nlm.nih.gov/pubmed/24765000
http://dx.doi.org/10.1107/S1600536814002955
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author Jan, Chin Yee
Shamsudin, Norzianah Binti Haji
Tan, Ai Ling
Young, David J.
Ng, Seik Weng
Tiekink, Edward R. T.
author_facet Jan, Chin Yee
Shamsudin, Norzianah Binti Haji
Tan, Ai Ling
Young, David J.
Ng, Seik Weng
Tiekink, Edward R. T.
author_sort Jan, Chin Yee
collection PubMed
description In the title compound, C(8)H(7)N(3)O(4) (systematic name: 4-nitro­benzene-1,2-dicarboxamide), each of the substituents is twisted out of the plane of the benzene ring to which it is attached [dihedral angles of 11.36 (2)° for the nitro group, and 60.89 (6) and 34.39 (6)° for the amide groups]. The amide groups are orientated to either side of the least-squares plane through the benzene ring with the amine groups being directed furthest apart. In the crystal, a three-dimensional architecture is established by a network of N—H⋯O hydrogen bonds.
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spelling pubmed-39985092014-04-24 4-Nitro­phthalamide Jan, Chin Yee Shamsudin, Norzianah Binti Haji Tan, Ai Ling Young, David J. Ng, Seik Weng Tiekink, Edward R. T. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(8)H(7)N(3)O(4) (systematic name: 4-nitro­benzene-1,2-dicarboxamide), each of the substituents is twisted out of the plane of the benzene ring to which it is attached [dihedral angles of 11.36 (2)° for the nitro group, and 60.89 (6) and 34.39 (6)° for the amide groups]. The amide groups are orientated to either side of the least-squares plane through the benzene ring with the amine groups being directed furthest apart. In the crystal, a three-dimensional architecture is established by a network of N—H⋯O hydrogen bonds. International Union of Crystallography 2014-02-15 /pmc/articles/PMC3998509/ /pubmed/24765000 http://dx.doi.org/10.1107/S1600536814002955 Text en © Jan et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jan, Chin Yee
Shamsudin, Norzianah Binti Haji
Tan, Ai Ling
Young, David J.
Ng, Seik Weng
Tiekink, Edward R. T.
4-Nitro­phthalamide
title 4-Nitro­phthalamide
title_full 4-Nitro­phthalamide
title_fullStr 4-Nitro­phthalamide
title_full_unstemmed 4-Nitro­phthalamide
title_short 4-Nitro­phthalamide
title_sort 4-nitro­phthalamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998509/
https://www.ncbi.nlm.nih.gov/pubmed/24765000
http://dx.doi.org/10.1107/S1600536814002955
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AT tiekinkedwardrt 4nitrophthalamide

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