(Z)-3-[2-(2,4-Di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3H)-one di­chloro­methane hemisolvate

In the title compound, 2C(14)H(8)N(4)O(6)·CH(2)Cl(2), the di­chloro­methane solvent mol­ecule resides on a crystallographic twofold axis. The mean plane of the phthaliso­imide ring is oriented at a dihedral angle of 32.93 (12)° with respect to the nitro-substituted benzene ring. An intra­molecular N...

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Detalles Bibliográficos
Autores principales: Agarwal, Palak, Mishra, Pragati, Gupta, Nikita, Neelam, Sahoo, Priyaranjan, Kumar, Satish
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998610/
https://www.ncbi.nlm.nih.gov/pubmed/24826131
http://dx.doi.org/10.1107/S1600536814004929
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author Agarwal, Palak
Mishra, Pragati
Gupta, Nikita
Neelam,
Sahoo, Priyaranjan
Kumar, Satish
author_facet Agarwal, Palak
Mishra, Pragati
Gupta, Nikita
Neelam,
Sahoo, Priyaranjan
Kumar, Satish
author_sort Agarwal, Palak
collection PubMed
description In the title compound, 2C(14)H(8)N(4)O(6)·CH(2)Cl(2), the di­chloro­methane solvent mol­ecule resides on a crystallographic twofold axis. The mean plane of the phthaliso­imide ring is oriented at a dihedral angle of 32.93 (12)° with respect to the nitro-substituted benzene ring. An intra­molecular N—H⋯O hydrogen bond occurs. The crystal packing features a short Cl⋯O halogen-bond inter­action [3.093 (3) Å].
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spelling pubmed-39986102014-05-13 (Z)-3-[2-(2,4-Di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3H)-one di­chloro­methane hemisolvate Agarwal, Palak Mishra, Pragati Gupta, Nikita Neelam, Sahoo, Priyaranjan Kumar, Satish Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, 2C(14)H(8)N(4)O(6)·CH(2)Cl(2), the di­chloro­methane solvent mol­ecule resides on a crystallographic twofold axis. The mean plane of the phthaliso­imide ring is oriented at a dihedral angle of 32.93 (12)° with respect to the nitro-substituted benzene ring. An intra­molecular N—H⋯O hydrogen bond occurs. The crystal packing features a short Cl⋯O halogen-bond inter­action [3.093 (3) Å]. International Union of Crystallography 2014-03-12 /pmc/articles/PMC3998610/ /pubmed/24826131 http://dx.doi.org/10.1107/S1600536814004929 Text en © Agarwal et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Agarwal, Palak
Mishra, Pragati
Gupta, Nikita
Neelam,
Sahoo, Priyaranjan
Kumar, Satish
(Z)-3-[2-(2,4-Di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3H)-one di­chloro­methane hemisolvate
title (Z)-3-[2-(2,4-Di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3H)-one di­chloro­methane hemisolvate
title_full (Z)-3-[2-(2,4-Di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3H)-one di­chloro­methane hemisolvate
title_fullStr (Z)-3-[2-(2,4-Di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3H)-one di­chloro­methane hemisolvate
title_full_unstemmed (Z)-3-[2-(2,4-Di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3H)-one di­chloro­methane hemisolvate
title_short (Z)-3-[2-(2,4-Di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3H)-one di­chloro­methane hemisolvate
title_sort (z)-3-[2-(2,4-di­nitro­phen­yl)hydrazin-1-yl­idene]isobenzo­furan-1(3h)-one di­chloro­methane hemisolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998610/
https://www.ncbi.nlm.nih.gov/pubmed/24826131
http://dx.doi.org/10.1107/S1600536814004929
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