(−)-Benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside

In the title compound, C(13)H(16)O(4), the six-membered ring of the sugar moiety shows a half-chair conformation. In the crystal, mol­ecules are connected via O—H⋯O hydrogen bonds, forming columns around twofold screw axes along the b-axis direction. There is a disorder of the benz­yloxy group, whic...

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Detalles Bibliográficos
Autores principales: Ohba, Shigeru, Okazaki, Hayato, Ueda, Yuji, Hanaya, Kengo, Shoji, Mitsuru, Sugai, Takeshi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4004438/
https://www.ncbi.nlm.nih.gov/pubmed/24860294
http://dx.doi.org/10.1107/S1600536813031140
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author Ohba, Shigeru
Okazaki, Hayato
Ueda, Yuji
Hanaya, Kengo
Shoji, Mitsuru
Sugai, Takeshi
author_facet Ohba, Shigeru
Okazaki, Hayato
Ueda, Yuji
Hanaya, Kengo
Shoji, Mitsuru
Sugai, Takeshi
author_sort Ohba, Shigeru
collection PubMed
description In the title compound, C(13)H(16)O(4), the six-membered ring of the sugar moiety shows a half-chair conformation. In the crystal, mol­ecules are connected via O—H⋯O hydrogen bonds, forming columns around twofold screw axes along the b-axis direction. There is a disorder of the benz­yloxy group, which has two possible orientations with the phenyl group lying on a common plane [site-occupancy factors = 0.589 (9) and 0.411 (9)].
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spelling pubmed-40044382014-05-23 (−)-Benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside Ohba, Shigeru Okazaki, Hayato Ueda, Yuji Hanaya, Kengo Shoji, Mitsuru Sugai, Takeshi Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(16)O(4), the six-membered ring of the sugar moiety shows a half-chair conformation. In the crystal, mol­ecules are connected via O—H⋯O hydrogen bonds, forming columns around twofold screw axes along the b-axis direction. There is a disorder of the benz­yloxy group, which has two possible orientations with the phenyl group lying on a common plane [site-occupancy factors = 0.589 (9) and 0.411 (9)]. International Union of Crystallography 2013-11-23 /pmc/articles/PMC4004438/ /pubmed/24860294 http://dx.doi.org/10.1107/S1600536813031140 Text en © Ohba et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ohba, Shigeru
Okazaki, Hayato
Ueda, Yuji
Hanaya, Kengo
Shoji, Mitsuru
Sugai, Takeshi
(−)-Benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside
title (−)-Benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside
title_full (−)-Benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside
title_fullStr (−)-Benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside
title_full_unstemmed (−)-Benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside
title_short (−)-Benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside
title_sort (−)-benzyl 2,3-dide­oxy-β-d-erythro-hex-2-eno­pyran­oside
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4004438/
https://www.ncbi.nlm.nih.gov/pubmed/24860294
http://dx.doi.org/10.1107/S1600536813031140
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AT sugaitakeshi benzyl23dideoxybderythrohex2enopyranoside

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