N-[Eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide

In the title compound, C(12)H(15)FN(2)O(2)S, the mol­ecule adopts a cis configuration of the fluoro­benzoyl group with respect to the thiono group about their C—N bond. The dihedral angle between the fluoro­benzoyl group and the thio­urea N(2)CS fragment is 69.60 (11)°. An intra­molecular N—H⋯O hydr...

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Autores principales: Awang, Nor Wahida., Hasbullah, Siti Aishah, Yusoff, Siti Fairus M., Yamin, Bohari M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4011211/
https://www.ncbi.nlm.nih.gov/pubmed/24860375
http://dx.doi.org/10.1107/S1600536814008174
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author Awang, Nor Wahida.
Hasbullah, Siti Aishah
Yusoff, Siti Fairus M.
Yamin, Bohari M.
author_facet Awang, Nor Wahida.
Hasbullah, Siti Aishah
Yusoff, Siti Fairus M.
Yamin, Bohari M.
author_sort Awang, Nor Wahida.
collection PubMed
description In the title compound, C(12)H(15)FN(2)O(2)S, the mol­ecule adopts a cis configuration of the fluoro­benzoyl group with respect to the thiono group about their C—N bond. The dihedral angle between the fluoro­benzoyl group and the thio­urea N(2)CS fragment is 69.60 (11)°. An intra­molecular N—H⋯O hydrogen bond occurs. In the crystal, mol­ecules form chains along the b-axis direction via O—H⋯S and C—H⋯O hydrogen bonds.
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spelling pubmed-40112112014-05-23 N-[Eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide Awang, Nor Wahida. Hasbullah, Siti Aishah Yusoff, Siti Fairus M. Yamin, Bohari M. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(12)H(15)FN(2)O(2)S, the mol­ecule adopts a cis configuration of the fluoro­benzoyl group with respect to the thiono group about their C—N bond. The dihedral angle between the fluoro­benzoyl group and the thio­urea N(2)CS fragment is 69.60 (11)°. An intra­molecular N—H⋯O hydrogen bond occurs. In the crystal, mol­ecules form chains along the b-axis direction via O—H⋯S and C—H⋯O hydrogen bonds. International Union of Crystallography 2014-04-18 /pmc/articles/PMC4011211/ /pubmed/24860375 http://dx.doi.org/10.1107/S1600536814008174 Text en © Awang et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Awang, Nor Wahida.
Hasbullah, Siti Aishah
Yusoff, Siti Fairus M.
Yamin, Bohari M.
N-[Eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide
title N-[Eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide
title_full N-[Eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide
title_fullStr N-[Eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide
title_full_unstemmed N-[Eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide
title_short N-[Eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide
title_sort n-[eth­yl(2-hy­droxy­eth­yl)carbamo­thio­yl]-3-fluoro­benzamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4011211/
https://www.ncbi.nlm.nih.gov/pubmed/24860375
http://dx.doi.org/10.1107/S1600536814008174
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AT yusoffsitifairusm nethyl2hydroxyethylcarbamothioyl3fluorobenzamide
AT yaminboharim nethyl2hydroxyethylcarbamothioyl3fluorobenzamide

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