4-Chloro-N′-[(E)-2-chloro­benzyl­idene]benzohydrazide monohydrate

The title compound, C(14)H(10)Cl(2)N(2)O·H(2)O, has a nearly planar extended conformation [C—N—N—C = −173.66 (15)°]. The dihedral angle between the aromatic rings is 4.6 (2)°. The water mol­ecules alternate with benzohydrazide mol­ecules in chains formed by O—H⋯O hydrogen bonds which run parallel to...

Descripción completa

Detalles Bibliográficos
Autores principales: Mague, Joel T., Mohamed, Shaaban K., Akkurt, Mehmet, Potgieter, Herman, Albayati, Mustafa R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4011300/
https://www.ncbi.nlm.nih.gov/pubmed/24860403
http://dx.doi.org/10.1107/S1600536814008885
_version_ 1782314792308965376
author Mague, Joel T.
Mohamed, Shaaban K.
Akkurt, Mehmet
Potgieter, Herman
Albayati, Mustafa R.
author_facet Mague, Joel T.
Mohamed, Shaaban K.
Akkurt, Mehmet
Potgieter, Herman
Albayati, Mustafa R.
author_sort Mague, Joel T.
collection PubMed
description The title compound, C(14)H(10)Cl(2)N(2)O·H(2)O, has a nearly planar extended conformation [C—N—N—C = −173.66 (15)°]. The dihedral angle between the aromatic rings is 4.6 (2)°. The water mol­ecules alternate with benzohydrazide mol­ecules in chains formed by O—H⋯O hydrogen bonds which run parallel to the a axis. These chains are linked to neighboring chains through N—H⋯O and C—H⋯O inter­actions, forming a layer parallel to (001).
format Online
Article
Text
id pubmed-4011300
institution National Center for Biotechnology Information
language English
publishDate 2014
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-40113002014-05-23 4-Chloro-N′-[(E)-2-chloro­benzyl­idene]benzohydrazide monohydrate Mague, Joel T. Mohamed, Shaaban K. Akkurt, Mehmet Potgieter, Herman Albayati, Mustafa R. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(10)Cl(2)N(2)O·H(2)O, has a nearly planar extended conformation [C—N—N—C = −173.66 (15)°]. The dihedral angle between the aromatic rings is 4.6 (2)°. The water mol­ecules alternate with benzohydrazide mol­ecules in chains formed by O—H⋯O hydrogen bonds which run parallel to the a axis. These chains are linked to neighboring chains through N—H⋯O and C—H⋯O inter­actions, forming a layer parallel to (001). International Union of Crystallography 2014-04-26 /pmc/articles/PMC4011300/ /pubmed/24860403 http://dx.doi.org/10.1107/S1600536814008885 Text en © Mague et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mague, Joel T.
Mohamed, Shaaban K.
Akkurt, Mehmet
Potgieter, Herman
Albayati, Mustafa R.
4-Chloro-N′-[(E)-2-chloro­benzyl­idene]benzohydrazide monohydrate
title 4-Chloro-N′-[(E)-2-chloro­benzyl­idene]benzohydrazide monohydrate
title_full 4-Chloro-N′-[(E)-2-chloro­benzyl­idene]benzohydrazide monohydrate
title_fullStr 4-Chloro-N′-[(E)-2-chloro­benzyl­idene]benzohydrazide monohydrate
title_full_unstemmed 4-Chloro-N′-[(E)-2-chloro­benzyl­idene]benzohydrazide monohydrate
title_short 4-Chloro-N′-[(E)-2-chloro­benzyl­idene]benzohydrazide monohydrate
title_sort 4-chloro-n′-[(e)-2-chloro­benzyl­idene]benzohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4011300/
https://www.ncbi.nlm.nih.gov/pubmed/24860403
http://dx.doi.org/10.1107/S1600536814008885
work_keys_str_mv AT maguejoelt 4chlorone2chlorobenzylidenebenzohydrazidemonohydrate
AT mohamedshaabank 4chlorone2chlorobenzylidenebenzohydrazidemonohydrate
AT akkurtmehmet 4chlorone2chlorobenzylidenebenzohydrazidemonohydrate
AT potgieterherman 4chlorone2chlorobenzylidenebenzohydrazidemonohydrate
AT albayatimustafar 4chlorone2chlorobenzylidenebenzohydrazidemonohydrate

Ejemplares similares