N,N′-(Propane-1,3-di­yl)dibenzo­thio­amide

The title compound, C(17)H(18)N(2)S(2), exhibits a trans–trans–trans–gauche(+) (tttg (+)) conformation with regard to the NH–CH(2)–CH(2)–CH(2)–NH bond sequence. In the crystal, mol­ecules are connected by N—H⋯S=C and C—H⋯S=C hydrogen bonds, forming a herringbone arrangement along the c-axis directio...

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Detalles Bibliográficos
Autores principales: Nagasawa, Masayuki, Sasanuma, Yuji, Masu, Hyuma
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051009/
https://www.ncbi.nlm.nih.gov/pubmed/24940226
http://dx.doi.org/10.1107/S160053681400974X
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author Nagasawa, Masayuki
Sasanuma, Yuji
Masu, Hyuma
author_facet Nagasawa, Masayuki
Sasanuma, Yuji
Masu, Hyuma
author_sort Nagasawa, Masayuki
collection PubMed
description The title compound, C(17)H(18)N(2)S(2), exhibits a trans–trans–trans–gauche(+) (tttg (+)) conformation with regard to the NH–CH(2)–CH(2)–CH(2)–NH bond sequence. In the crystal, mol­ecules are connected by N—H⋯S=C and C—H⋯S=C hydrogen bonds, forming a herringbone arrangement along the c-axis direction. The two thioamide groups make dihedral angles of 43.0 (2) and 33.1 (2)° with the adjacent phenyl rings.
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spelling pubmed-40510092014-06-17 N,N′-(Propane-1,3-di­yl)dibenzo­thio­amide Nagasawa, Masayuki Sasanuma, Yuji Masu, Hyuma Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(18)N(2)S(2), exhibits a trans–trans–trans–gauche(+) (tttg (+)) conformation with regard to the NH–CH(2)–CH(2)–CH(2)–NH bond sequence. In the crystal, mol­ecules are connected by N—H⋯S=C and C—H⋯S=C hydrogen bonds, forming a herringbone arrangement along the c-axis direction. The two thioamide groups make dihedral angles of 43.0 (2) and 33.1 (2)° with the adjacent phenyl rings. International Union of Crystallography 2014-05-03 /pmc/articles/PMC4051009/ /pubmed/24940226 http://dx.doi.org/10.1107/S160053681400974X Text en © Nagasawa et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Nagasawa, Masayuki
Sasanuma, Yuji
Masu, Hyuma
N,N′-(Propane-1,3-di­yl)dibenzo­thio­amide
title N,N′-(Propane-1,3-di­yl)dibenzo­thio­amide
title_full N,N′-(Propane-1,3-di­yl)dibenzo­thio­amide
title_fullStr N,N′-(Propane-1,3-di­yl)dibenzo­thio­amide
title_full_unstemmed N,N′-(Propane-1,3-di­yl)dibenzo­thio­amide
title_short N,N′-(Propane-1,3-di­yl)dibenzo­thio­amide
title_sort n,n′-(propane-1,3-di­yl)dibenzo­thio­amide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051009/
https://www.ncbi.nlm.nih.gov/pubmed/24940226
http://dx.doi.org/10.1107/S160053681400974X
work_keys_str_mv AT nagasawamasayuki nnpropane13diyldibenzothioamide
AT sasanumayuji nnpropane13diyldibenzothioamide
AT masuhyuma nnpropane13diyldibenzothioamide

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