(3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate

In the title compound, C(16)H(10)N(4)O(2)·0.17H(2)O, prepared by the one-step condensation reaction of isatin with hydrazine hydrate under microwave irradiation, the complete organic mol­ecule is generated by crystallographic inversion symmetry and therefore exists in an S-trans conformation. In the...

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Detalles Bibliográficos
Autores principales: Liu, Yong-Hong, Zhao, Lei, Liu, Ming-Xuan, Lin, Hai, Li, Jing-Jing
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051016/
https://www.ncbi.nlm.nih.gov/pubmed/24940290
http://dx.doi.org/10.1107/S1600536814011805
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author Liu, Yong-Hong
Zhao, Lei
Liu, Ming-Xuan
Lin, Hai
Li, Jing-Jing
author_facet Liu, Yong-Hong
Zhao, Lei
Liu, Ming-Xuan
Lin, Hai
Li, Jing-Jing
author_sort Liu, Yong-Hong
collection PubMed
description In the title compound, C(16)H(10)N(4)O(2)·0.17H(2)O, prepared by the one-step condensation reaction of isatin with hydrazine hydrate under microwave irradiation, the complete organic mol­ecule is generated by crystallographic inversion symmetry and therefore exists in an S-trans conformation. In the crystal, mol­ecules are linked by N—H⋯O hydrogen bonds, generating a three-dimensional framework with [001] channels, which are occupied by the disordered water mol­ecules.
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spelling pubmed-40510162014-06-17 (3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate Liu, Yong-Hong Zhao, Lei Liu, Ming-Xuan Lin, Hai Li, Jing-Jing Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(10)N(4)O(2)·0.17H(2)O, prepared by the one-step condensation reaction of isatin with hydrazine hydrate under microwave irradiation, the complete organic mol­ecule is generated by crystallographic inversion symmetry and therefore exists in an S-trans conformation. In the crystal, mol­ecules are linked by N—H⋯O hydrogen bonds, generating a three-dimensional framework with [001] channels, which are occupied by the disordered water mol­ecules. International Union of Crystallography 2014-05-31 /pmc/articles/PMC4051016/ /pubmed/24940290 http://dx.doi.org/10.1107/S1600536814011805 Text en © Liu et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Yong-Hong
Zhao, Lei
Liu, Ming-Xuan
Lin, Hai
Li, Jing-Jing
(3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate
title (3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate
title_full (3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate
title_fullStr (3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate
title_full_unstemmed (3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate
title_short (3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate
title_sort (3z)-3-[(z)-2-(2-oxoindolin-3-yl­idene)hydrazin-1-yl­idene]indolin-2-one 0.17-hydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051016/
https://www.ncbi.nlm.nih.gov/pubmed/24940290
http://dx.doi.org/10.1107/S1600536814011805
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