tert-Butyl N-[2-(N-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate

The title compound, C(18)H(30)N(2)O(5)S, was synthesized by the reaction of tert-butyl 2-(iso­butyl­amino)­ethyl­carbamate with p-meth­oxy­phenyl­sulfonyl chloride. In the mol­ecule, two intra­molecular C—H⋯O hydrogen bonds are observed. In the crystal, mol­ecules are linked by N—H⋯O hydrogen bonds...

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Detalles Bibliográficos
Autores principales: Bai, Xiao-Guang, Wang, Ju-Xian
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051064/
https://www.ncbi.nlm.nih.gov/pubmed/24940254
http://dx.doi.org/10.1107/S1600536814009143
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author Bai, Xiao-Guang
Wang, Ju-Xian
author_facet Bai, Xiao-Guang
Wang, Ju-Xian
author_sort Bai, Xiao-Guang
collection PubMed
description The title compound, C(18)H(30)N(2)O(5)S, was synthesized by the reaction of tert-butyl 2-(iso­butyl­amino)­ethyl­carbamate with p-meth­oxy­phenyl­sulfonyl chloride. In the mol­ecule, two intra­molecular C—H⋯O hydrogen bonds are observed. In the crystal, mol­ecules are linked by N—H⋯O hydrogen bonds involving the imino group N atom and the ester group O atom into chains running parallel to the b axis. The chains are further connected by C—H⋯O hydrogen bonds, forming layers parallel to the bc plane.
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spelling pubmed-40510642014-06-17 tert-Butyl N-[2-(N-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate Bai, Xiao-Guang Wang, Ju-Xian Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(30)N(2)O(5)S, was synthesized by the reaction of tert-butyl 2-(iso­butyl­amino)­ethyl­carbamate with p-meth­oxy­phenyl­sulfonyl chloride. In the mol­ecule, two intra­molecular C—H⋯O hydrogen bonds are observed. In the crystal, mol­ecules are linked by N—H⋯O hydrogen bonds involving the imino group N atom and the ester group O atom into chains running parallel to the b axis. The chains are further connected by C—H⋯O hydrogen bonds, forming layers parallel to the bc plane. International Union of Crystallography 2014-05-17 /pmc/articles/PMC4051064/ /pubmed/24940254 http://dx.doi.org/10.1107/S1600536814009143 Text en © Bai and Wang 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Bai, Xiao-Guang
Wang, Ju-Xian
tert-Butyl N-[2-(N-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate
title tert-Butyl N-[2-(N-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate
title_full tert-Butyl N-[2-(N-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate
title_fullStr tert-Butyl N-[2-(N-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate
title_full_unstemmed tert-Butyl N-[2-(N-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate
title_short tert-Butyl N-[2-(N-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate
title_sort tert-butyl n-[2-(n-isobutyl-4-meth­oxy­benzene­sulfonamido)­eth­yl]carbamate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051064/
https://www.ncbi.nlm.nih.gov/pubmed/24940254
http://dx.doi.org/10.1107/S1600536814009143
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