N-Ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide

In the title compound, C(15)H(17)N(3)OS, the dihedral angle between the mean planes of the 2-hy­droxy­napthyl ring system and the hydrazinecarbo­thio­amide group is 73.7 (3)°. In the crystal, weak O—H⋯S and C—H⋯O inter­actions and π–π stacking inter­actions involving one of the hy­droxy­napthyl ring...

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Detalles Bibliográficos
Autores principales: Anderson, Brian J., Shalit, Zachary A., Jasinski, Jerry P.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051082/
https://www.ncbi.nlm.nih.gov/pubmed/24940298
http://dx.doi.org/10.1107/S1600536814012057
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author Anderson, Brian J.
Shalit, Zachary A.
Jasinski, Jerry P.
author_facet Anderson, Brian J.
Shalit, Zachary A.
Jasinski, Jerry P.
author_sort Anderson, Brian J.
collection PubMed
description In the title compound, C(15)H(17)N(3)OS, the dihedral angle between the mean planes of the 2-hy­droxy­napthyl ring system and the hydrazinecarbo­thio­amide group is 73.7 (3)°. In the crystal, weak O—H⋯S and C—H⋯O inter­actions and π–π stacking inter­actions involving one of the hy­droxy­napthyl rings with a centroid–centroid distance of 3.6648 (14) Å are observed, forming infinite chains along [010]. In addition, N—H⋯S inter­actions occur.
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spelling pubmed-40510822014-06-17 N-Ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide Anderson, Brian J. Shalit, Zachary A. Jasinski, Jerry P. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(17)N(3)OS, the dihedral angle between the mean planes of the 2-hy­droxy­napthyl ring system and the hydrazinecarbo­thio­amide group is 73.7 (3)°. In the crystal, weak O—H⋯S and C—H⋯O inter­actions and π–π stacking inter­actions involving one of the hy­droxy­napthyl rings with a centroid–centroid distance of 3.6648 (14) Å are observed, forming infinite chains along [010]. In addition, N—H⋯S inter­actions occur. International Union of Crystallography 2014-05-31 /pmc/articles/PMC4051082/ /pubmed/24940298 http://dx.doi.org/10.1107/S1600536814012057 Text en © Anderson et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Anderson, Brian J.
Shalit, Zachary A.
Jasinski, Jerry P.
N-Ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide
title N-Ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide
title_full N-Ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide
title_fullStr N-Ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide
title_full_unstemmed N-Ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide
title_short N-Ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide
title_sort n-ethyl-2-[1-(2-hy­droxy­naphthalen-1-yl)ethyl­idene]hydrazinecarbo­thio­amide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051082/
https://www.ncbi.nlm.nih.gov/pubmed/24940298
http://dx.doi.org/10.1107/S1600536814012057
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AT jasinskijerryp nethyl212hydroxynaphthalen1ylethylidenehydrazinecarbothioamide

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