2-Benzoyl-4-chloro­aniline thio­semi­carbazone

In the title compound, C(14)H(13)ClN(4)S, obtained from a reaction of 2-benzoyl-4-chloro­aniline with thio­semicarbazide in ethanol, the dihedral angle between the aromatic rings is 81.31 (13)°. In the crystal, the mol­ecules are linked by three N—H⋯S hydrogen bonds, forming centrosymmetric rings wi...

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Detalles Bibliográficos
Autores principales: Bandeira, Katlen C. T., Bresolin, Leandro, Lehmann, Ueslei Z., Zambiazi, Priscilla J., de Oliveira, Adriano Bof
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051094/
https://www.ncbi.nlm.nih.gov/pubmed/24940260
http://dx.doi.org/10.1107/S1600536814011027
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author Bandeira, Katlen C. T.
Bresolin, Leandro
Lehmann, Ueslei Z.
Zambiazi, Priscilla J.
de Oliveira, Adriano Bof
author_facet Bandeira, Katlen C. T.
Bresolin, Leandro
Lehmann, Ueslei Z.
Zambiazi, Priscilla J.
de Oliveira, Adriano Bof
author_sort Bandeira, Katlen C. T.
collection PubMed
description In the title compound, C(14)H(13)ClN(4)S, obtained from a reaction of 2-benzoyl-4-chloro­aniline with thio­semicarbazide in ethanol, the dihedral angle between the aromatic rings is 81.31 (13)°. In the crystal, the mol­ecules are linked by three N—H⋯S hydrogen bonds, forming centrosymmetric rings with set-graph motif R (2) (2)(8) and R (2) (2)(18), and resulting in the formation of a two-dimensional network lying parallel to (010).
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spelling pubmed-40510942014-06-17 2-Benzoyl-4-chloro­aniline thio­semi­carbazone Bandeira, Katlen C. T. Bresolin, Leandro Lehmann, Ueslei Z. Zambiazi, Priscilla J. de Oliveira, Adriano Bof Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(13)ClN(4)S, obtained from a reaction of 2-benzoyl-4-chloro­aniline with thio­semicarbazide in ethanol, the dihedral angle between the aromatic rings is 81.31 (13)°. In the crystal, the mol­ecules are linked by three N—H⋯S hydrogen bonds, forming centrosymmetric rings with set-graph motif R (2) (2)(8) and R (2) (2)(18), and resulting in the formation of a two-dimensional network lying parallel to (010). International Union of Crystallography 2014-05-17 /pmc/articles/PMC4051094/ /pubmed/24940260 http://dx.doi.org/10.1107/S1600536814011027 Text en © Bandeira et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Bandeira, Katlen C. T.
Bresolin, Leandro
Lehmann, Ueslei Z.
Zambiazi, Priscilla J.
de Oliveira, Adriano Bof
2-Benzoyl-4-chloro­aniline thio­semi­carbazone
title 2-Benzoyl-4-chloro­aniline thio­semi­carbazone
title_full 2-Benzoyl-4-chloro­aniline thio­semi­carbazone
title_fullStr 2-Benzoyl-4-chloro­aniline thio­semi­carbazone
title_full_unstemmed 2-Benzoyl-4-chloro­aniline thio­semi­carbazone
title_short 2-Benzoyl-4-chloro­aniline thio­semi­carbazone
title_sort 2-benzoyl-4-chloro­aniline thio­semi­carbazone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4051094/
https://www.ncbi.nlm.nih.gov/pubmed/24940260
http://dx.doi.org/10.1107/S1600536814011027
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