Quantitative analysis of trigonelline in some Annona species by proton NMR spectroscopy

A quantitative (1)H NMR method (qHNMR) was used to measure the trigonelline content in the leaves of six species of the Annona genus. The methodology employed compared the intensities of the signals at δ 9.14 (H-2) and δ 0.00, the internal standard TSP-d(4). This measuring method was able to establi...

Descripción completa

Detalles Bibliográficos
Autores principales: Machado, Alan Rodrigues Teixeira, Lage, Gisele Avelar, Medeiros, Felipe da Silva, de Souza Filho, José Dias, Pimenta, Lúcia Pinheiro Santos
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer Berlin Heidelberg 2013
Materias:
Short Communication
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4131578/
http://dx.doi.org/10.1007/s13659-013-0051-6
_version_ 1782330484304379904
author Machado, Alan Rodrigues Teixeira
Lage, Gisele Avelar
Medeiros, Felipe da Silva
de Souza Filho, José Dias
Pimenta, Lúcia Pinheiro Santos
author_facet Machado, Alan Rodrigues Teixeira
Lage, Gisele Avelar
Medeiros, Felipe da Silva
de Souza Filho, José Dias
Pimenta, Lúcia Pinheiro Santos
author_sort Machado, Alan Rodrigues Teixeira
collection PubMed
description A quantitative (1)H NMR method (qHNMR) was used to measure the trigonelline content in the leaves of six species of the Annona genus. The methodology employed compared the intensities of the signals at δ 9.14 (H-2) and δ 0.00, the internal standard TSP-d(4). This measuring method was able to establish the concentration of trigonelline in the range from 0.67 to 10.04 mg·g(−1) depending on the investigated extract. [Image: see text]
format Online
Article
Text
id pubmed-4131578
institution National Center for Biotechnology Information
language English
publishDate 2013
publisher Springer Berlin Heidelberg
record_format MEDLINE/PubMed
spelling pubmed-41315782014-08-20 Quantitative analysis of trigonelline in some Annona species by proton NMR spectroscopy Machado, Alan Rodrigues Teixeira Lage, Gisele Avelar Medeiros, Felipe da Silva de Souza Filho, José Dias Pimenta, Lúcia Pinheiro Santos Nat Prod Bioprospect Short Communication A quantitative (1)H NMR method (qHNMR) was used to measure the trigonelline content in the leaves of six species of the Annona genus. The methodology employed compared the intensities of the signals at δ 9.14 (H-2) and δ 0.00, the internal standard TSP-d(4). This measuring method was able to establish the concentration of trigonelline in the range from 0.67 to 10.04 mg·g(−1) depending on the investigated extract. [Image: see text] Springer Berlin Heidelberg 2013-07-31 /pmc/articles/PMC4131578/ http://dx.doi.org/10.1007/s13659-013-0051-6 Text en © The Author(s) 2013 https://creativecommons.org/licenses/by/4.0/ This article is published under license to BioMed Central Ltd. Open Access This article is distributed under the terms of the Creative Commons Attribution License which permits any use, distribution and reproduction in any medium, provided the original author(s) and source are credited.
spellingShingle Short Communication
Machado, Alan Rodrigues Teixeira
Lage, Gisele Avelar
Medeiros, Felipe da Silva
de Souza Filho, José Dias
Pimenta, Lúcia Pinheiro Santos
Quantitative analysis of trigonelline in some Annona species by proton NMR spectroscopy
title Quantitative analysis of trigonelline in some Annona species by proton NMR spectroscopy
title_full Quantitative analysis of trigonelline in some Annona species by proton NMR spectroscopy
title_fullStr Quantitative analysis of trigonelline in some Annona species by proton NMR spectroscopy
title_full_unstemmed Quantitative analysis of trigonelline in some Annona species by proton NMR spectroscopy
title_short Quantitative analysis of trigonelline in some Annona species by proton NMR spectroscopy
title_sort quantitative analysis of trigonelline in some annona species by proton nmr spectroscopy
topic Short Communication
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4131578/
http://dx.doi.org/10.1007/s13659-013-0051-6
work_keys_str_mv AT machadoalanrodriguesteixeira quantitativeanalysisoftrigonellineinsomeannonaspeciesbyprotonnmrspectroscopy
AT lagegiseleavelar quantitativeanalysisoftrigonellineinsomeannonaspeciesbyprotonnmrspectroscopy
AT medeirosfelipedasilva quantitativeanalysisoftrigonellineinsomeannonaspeciesbyprotonnmrspectroscopy
AT desouzafilhojosedias quantitativeanalysisoftrigonellineinsomeannonaspeciesbyprotonnmrspectroscopy
AT pimentaluciapinheirosantos quantitativeanalysisoftrigonellineinsomeannonaspeciesbyprotonnmrspectroscopy

Ejemplares similares