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Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol
A facile one-pot approach for synthesis of gold nanoparticles with narrow size distribution and good stability was presented by reducing chloroauric acid with a polysaccharide, konjac glucomannan (KGM) in alkaline solution, which is green and economically viable. Here, KGM served both as reducing ag...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Springer
2014
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4145362/ https://www.ncbi.nlm.nih.gov/pubmed/25177220 http://dx.doi.org/10.1186/1556-276X-9-404 |
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author | Gao, Zhao Su, Rongxin Huang, Renliang Qi, Wei He, Zhimin |
author_facet | Gao, Zhao Su, Rongxin Huang, Renliang Qi, Wei He, Zhimin |
author_sort | Gao, Zhao |
collection | PubMed |
description | A facile one-pot approach for synthesis of gold nanoparticles with narrow size distribution and good stability was presented by reducing chloroauric acid with a polysaccharide, konjac glucomannan (KGM) in alkaline solution, which is green and economically viable. Here, KGM served both as reducing agent and stabilizer. The effects of KGM on the formation and stabilization of as-synthesized gold nanoparticles were studied systematically by a combination of UV-visible (UV-vis) absorption spectroscopy, transmission electron microscopy, X-ray diffraction, dynamic light scattering, and Fourier transform infrared spectroscopy. Furthermore, the gold nanoparticles exhibited a notable catalytic activity toward the reduction of 4-nitrophenol to 4-aminophenol. |
format | Online Article Text |
id | pubmed-4145362 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2014 |
publisher | Springer |
record_format | MEDLINE/PubMed |
spelling | pubmed-41453622014-08-29 Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol Gao, Zhao Su, Rongxin Huang, Renliang Qi, Wei He, Zhimin Nanoscale Res Lett Nano Express A facile one-pot approach for synthesis of gold nanoparticles with narrow size distribution and good stability was presented by reducing chloroauric acid with a polysaccharide, konjac glucomannan (KGM) in alkaline solution, which is green and economically viable. Here, KGM served both as reducing agent and stabilizer. The effects of KGM on the formation and stabilization of as-synthesized gold nanoparticles were studied systematically by a combination of UV-visible (UV-vis) absorption spectroscopy, transmission electron microscopy, X-ray diffraction, dynamic light scattering, and Fourier transform infrared spectroscopy. Furthermore, the gold nanoparticles exhibited a notable catalytic activity toward the reduction of 4-nitrophenol to 4-aminophenol. Springer 2014-08-20 /pmc/articles/PMC4145362/ /pubmed/25177220 http://dx.doi.org/10.1186/1556-276X-9-404 Text en Copyright © 2014 Gao et al.; licensee Springer. http://creativecommons.org/licenses/by/4.0 This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly credited. |
spellingShingle | Nano Express Gao, Zhao Su, Rongxin Huang, Renliang Qi, Wei He, Zhimin Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol |
title | Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol |
title_full | Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol |
title_fullStr | Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol |
title_full_unstemmed | Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol |
title_short | Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol |
title_sort | glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol |
topic | Nano Express |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4145362/ https://www.ncbi.nlm.nih.gov/pubmed/25177220 http://dx.doi.org/10.1186/1556-276X-9-404 |
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