Cargando…

High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector

Coherent (X-ray) diffractive imaging (CDI) is an increasingly popular form of X-ray microscopy, mainly due to its potential to produce high-resolution images and the lack of an objective lens between the sample and its corresponding imaging detector. One challenge, however, is that very high dynamic...

Descripción completa

Detalles Bibliográficos
Autores principales: Giewekemeyer, Klaus, Philipp, Hugh T., Wilke, Robin N., Aquila, Andrew, Osterhoff, Markus, Tate, Mark W., Shanks, Katherine S., Zozulya, Alexey V., Salditt, Tim, Gruner, Sol M., Mancuso, Adrian P.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4151683/
https://www.ncbi.nlm.nih.gov/pubmed/25178008
http://dx.doi.org/10.1107/S1600577514013411
_version_ 1782333048948260864
author Giewekemeyer, Klaus
Philipp, Hugh T.
Wilke, Robin N.
Aquila, Andrew
Osterhoff, Markus
Tate, Mark W.
Shanks, Katherine S.
Zozulya, Alexey V.
Salditt, Tim
Gruner, Sol M.
Mancuso, Adrian P.
author_facet Giewekemeyer, Klaus
Philipp, Hugh T.
Wilke, Robin N.
Aquila, Andrew
Osterhoff, Markus
Tate, Mark W.
Shanks, Katherine S.
Zozulya, Alexey V.
Salditt, Tim
Gruner, Sol M.
Mancuso, Adrian P.
author_sort Giewekemeyer, Klaus
collection PubMed
description Coherent (X-ray) diffractive imaging (CDI) is an increasingly popular form of X-ray microscopy, mainly due to its potential to produce high-resolution images and the lack of an objective lens between the sample and its corresponding imaging detector. One challenge, however, is that very high dynamic range diffraction data must be collected to produce both quantitative and high-resolution images. In this work, hard X-ray ptychographic coherent diffractive imaging has been performed at the P10 beamline of the PETRA III synchrotron to demonstrate the potential of a very wide dynamic range imaging X-ray detector (the Mixed-Mode Pixel Array Detector, or MM-PAD). The detector is capable of single photon detection, detecting fluxes exceeding 1 × 10(8) 8-keV photons pixel(−1) s(−1), and framing at 1 kHz. A ptychographic reconstruction was performed using a peak focal intensity on the order of 1 × 10(10) photons µm(−2) s(−1) within an area of approximately 325 nm × 603 nm. This was done without need of a beam stop and with a very modest attenuation, while ‘still’ images of the empty beam far-field intensity were recorded without any attenuation. The treatment of the detector frames and CDI methodology for reconstruction of non-sensitive detector regions, partially also extending the active detector area, are described.
format Online
Article
Text
id pubmed-4151683
institution National Center for Biotechnology Information
language English
publishDate 2014
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-41516832014-09-23 High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector Giewekemeyer, Klaus Philipp, Hugh T. Wilke, Robin N. Aquila, Andrew Osterhoff, Markus Tate, Mark W. Shanks, Katherine S. Zozulya, Alexey V. Salditt, Tim Gruner, Sol M. Mancuso, Adrian P. J Synchrotron Radiat Research Papers Coherent (X-ray) diffractive imaging (CDI) is an increasingly popular form of X-ray microscopy, mainly due to its potential to produce high-resolution images and the lack of an objective lens between the sample and its corresponding imaging detector. One challenge, however, is that very high dynamic range diffraction data must be collected to produce both quantitative and high-resolution images. In this work, hard X-ray ptychographic coherent diffractive imaging has been performed at the P10 beamline of the PETRA III synchrotron to demonstrate the potential of a very wide dynamic range imaging X-ray detector (the Mixed-Mode Pixel Array Detector, or MM-PAD). The detector is capable of single photon detection, detecting fluxes exceeding 1 × 10(8) 8-keV photons pixel(−1) s(−1), and framing at 1 kHz. A ptychographic reconstruction was performed using a peak focal intensity on the order of 1 × 10(10) photons µm(−2) s(−1) within an area of approximately 325 nm × 603 nm. This was done without need of a beam stop and with a very modest attenuation, while ‘still’ images of the empty beam far-field intensity were recorded without any attenuation. The treatment of the detector frames and CDI methodology for reconstruction of non-sensitive detector regions, partially also extending the active detector area, are described. International Union of Crystallography 2014-08-07 /pmc/articles/PMC4151683/ /pubmed/25178008 http://dx.doi.org/10.1107/S1600577514013411 Text en © Klaus Giewekemeyer et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Giewekemeyer, Klaus
Philipp, Hugh T.
Wilke, Robin N.
Aquila, Andrew
Osterhoff, Markus
Tate, Mark W.
Shanks, Katherine S.
Zozulya, Alexey V.
Salditt, Tim
Gruner, Sol M.
Mancuso, Adrian P.
High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector
title High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector
title_full High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector
title_fullStr High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector
title_full_unstemmed High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector
title_short High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector
title_sort high-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4151683/
https://www.ncbi.nlm.nih.gov/pubmed/25178008
http://dx.doi.org/10.1107/S1600577514013411
work_keys_str_mv AT giewekemeyerklaus highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT philipphught highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT wilkerobinn highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT aquilaandrew highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT osterhoffmarkus highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT tatemarkw highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT shankskatherines highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT zozulyaalexeyv highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT salditttim highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT grunersolm highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector
AT mancusoadrianp highdynamicrangecoherentdiffractiveimagingptychographyusingthemixedmodepixelarraydetector