Di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate

The title compound, C(14)H(28)N(2)O(5)S, was synthesized by the reaction of 2-[(methyl­sulfan­yl)meth­yl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen bonds into supra­molecular chains propagating along the b-axis direction...

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Detalles Bibliográficos
Autores principales: Bai, Xiao-Guang, Yang, Xiao-Yu, Wang, Ju-Xian
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4158484/
https://www.ncbi.nlm.nih.gov/pubmed/25249896
http://dx.doi.org/10.1107/S1600536814015062
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author Bai, Xiao-Guang
Yang, Xiao-Yu
Wang, Ju-Xian
author_facet Bai, Xiao-Guang
Yang, Xiao-Yu
Wang, Ju-Xian
author_sort Bai, Xiao-Guang
collection PubMed
description The title compound, C(14)H(28)N(2)O(5)S, was synthesized by the reaction of 2-[(methyl­sulfan­yl)meth­yl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen bonds into supra­molecular chains propagating along the b-axis direction.
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spelling pubmed-41584842014-09-23 Di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate Bai, Xiao-Guang Yang, Xiao-Yu Wang, Ju-Xian Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(28)N(2)O(5)S, was synthesized by the reaction of 2-[(methyl­sulfan­yl)meth­yl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen bonds into supra­molecular chains propagating along the b-axis direction. International Union of Crystallography 2014-07-02 /pmc/articles/PMC4158484/ /pubmed/25249896 http://dx.doi.org/10.1107/S1600536814015062 Text en © Bai et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Bai, Xiao-Guang
Yang, Xiao-Yu
Wang, Ju-Xian
Di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate
title Di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate
title_full Di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate
title_fullStr Di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate
title_full_unstemmed Di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate
title_short Di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate
title_sort di-tert-butyl 1-[2-hy­droxy-3-(methyl­sulfan­yl)prop­yl]hydrazine-1,2-di­carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4158484/
https://www.ncbi.nlm.nih.gov/pubmed/25249896
http://dx.doi.org/10.1107/S1600536814015062
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AT wangjuxian ditertbutyl12hydroxy3methylsulfanylpropylhydrazine12dicarboxylate

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