4-Hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone

In the crystal structure of the title compound, C(11)H(15)N(3)O(2)S, the C—N—N—C and C—N—C—C torsion angles involving the benzene ring and ethyl group are 11.91 (15) and 99.4 (2)°, respectively. An intra­molecular N—H⋯N hydrogen bond is observed. In the crystal, mol­ecules are linked via N—H⋯O and N...

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Autores principales: de Oliveira, Adriano Bof, Beck, Johannes, Daniels, Jörg, Feitosa, Bárbara Regina Santos
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4158485/
https://www.ncbi.nlm.nih.gov/pubmed/25249915
http://dx.doi.org/10.1107/S1600536814016018
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author de Oliveira, Adriano Bof
Beck, Johannes
Daniels, Jörg
Feitosa, Bárbara Regina Santos
author_facet de Oliveira, Adriano Bof
Beck, Johannes
Daniels, Jörg
Feitosa, Bárbara Regina Santos
author_sort de Oliveira, Adriano Bof
collection PubMed
description In the crystal structure of the title compound, C(11)H(15)N(3)O(2)S, the C—N—N—C and C—N—C—C torsion angles involving the benzene ring and ethyl group are 11.91 (15) and 99.4 (2)°, respectively. An intra­molecular N—H⋯N hydrogen bond is observed. In the crystal, mol­ecules are linked via N—H⋯O and N—H⋯S hydrogen bonds into a three-dimensional hydrogen bonded network. Finally, the molecules show a herringbone arrangement when viewed along the a axis.
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spelling pubmed-41584852014-09-23 4-Hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone de Oliveira, Adriano Bof Beck, Johannes Daniels, Jörg Feitosa, Bárbara Regina Santos Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(11)H(15)N(3)O(2)S, the C—N—N—C and C—N—C—C torsion angles involving the benzene ring and ethyl group are 11.91 (15) and 99.4 (2)°, respectively. An intra­molecular N—H⋯N hydrogen bond is observed. In the crystal, mol­ecules are linked via N—H⋯O and N—H⋯S hydrogen bonds into a three-dimensional hydrogen bonded network. Finally, the molecules show a herringbone arrangement when viewed along the a axis. International Union of Crystallography 2014-07-17 /pmc/articles/PMC4158485/ /pubmed/25249915 http://dx.doi.org/10.1107/S1600536814016018 Text en © Oliveira et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
de Oliveira, Adriano Bof
Beck, Johannes
Daniels, Jörg
Feitosa, Bárbara Regina Santos
4-Hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone
title 4-Hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone
title_full 4-Hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone
title_fullStr 4-Hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone
title_full_unstemmed 4-Hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone
title_short 4-Hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone
title_sort 4-hy­droxy-3-meth­oxy­benzaldehyde 4-ethyl­thio­semicarbazone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4158485/
https://www.ncbi.nlm.nih.gov/pubmed/25249915
http://dx.doi.org/10.1107/S1600536814016018
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AT feitosabarbarareginasantos 4hydroxy3methoxybenzaldehyde4ethylthiosemicarbazone

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