5-Hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (HNBATSC)

The asymmetric unit of the title compound, C(8)H(8)N(4)O(3)S, consists of two independent mol­ecules. Each mol­ecule is approximately planar with dihedral angles of 8.71 (3) and 1.50 (2)° between the aromatic ring and the thio­semicarbazide moiety while the NO(2) group makes dihedral angles of 29.27...

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Autores principales: Reddy, M. Sivasankar, Sarala, Y., Jagadeesh, M., Das, Samar K., Ammireddy, Varada Reddy
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4158534/
https://www.ncbi.nlm.nih.gov/pubmed/25249898
http://dx.doi.org/10.1107/S1600536814015098
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author Reddy, M. Sivasankar
Sarala, Y.
Jagadeesh, M.
Das, Samar K.
Ammireddy, Varada Reddy
author_facet Reddy, M. Sivasankar
Sarala, Y.
Jagadeesh, M.
Das, Samar K.
Ammireddy, Varada Reddy
author_sort Reddy, M. Sivasankar
collection PubMed
description The asymmetric unit of the title compound, C(8)H(8)N(4)O(3)S, consists of two independent mol­ecules. Each mol­ecule is approximately planar with dihedral angles of 8.71 (3) and 1.50 (2)° between the aromatic ring and the thio­semicarbazide moiety while the NO(2) group makes dihedral angles of 29.27 (3) and 17.78 (3)° with the benzene ring. In the crystal, the molecules are linked by N—H⋯S, O—H⋯O and N—H⋯O hydrogen bonds, forming two-dimensional networks parallel to (100).
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spelling pubmed-41585342014-09-23 5-Hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (HNBATSC) Reddy, M. Sivasankar Sarala, Y. Jagadeesh, M. Das, Samar K. Ammireddy, Varada Reddy Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(8)H(8)N(4)O(3)S, consists of two independent mol­ecules. Each mol­ecule is approximately planar with dihedral angles of 8.71 (3) and 1.50 (2)° between the aromatic ring and the thio­semicarbazide moiety while the NO(2) group makes dihedral angles of 29.27 (3) and 17.78 (3)° with the benzene ring. In the crystal, the molecules are linked by N—H⋯S, O—H⋯O and N—H⋯O hydrogen bonds, forming two-dimensional networks parallel to (100). International Union of Crystallography 2014-07-02 /pmc/articles/PMC4158534/ /pubmed/25249898 http://dx.doi.org/10.1107/S1600536814015098 Text en © Reddy et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Reddy, M. Sivasankar
Sarala, Y.
Jagadeesh, M.
Das, Samar K.
Ammireddy, Varada Reddy
5-Hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (HNBATSC)
title 5-Hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (HNBATSC)
title_full 5-Hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (HNBATSC)
title_fullStr 5-Hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (HNBATSC)
title_full_unstemmed 5-Hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (HNBATSC)
title_short 5-Hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (HNBATSC)
title_sort 5-hy­droxy-2-nitro­benzaldehyde thio­semicarbazone (hnbatsc)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4158534/
https://www.ncbi.nlm.nih.gov/pubmed/25249898
http://dx.doi.org/10.1107/S1600536814015098
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