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Scalable synthesis of 5,11-diethynylated indeno[1,2-b]fluorene-6,12-diones and exploration of their solid state packing

We report a new synthetic route to 5,11-disubstituted indeno[1,2-b]fluorene-6,12-diones that is amenable to larger scale reactions, allowing for the preparation of gram amounts of material. With this new methodology, we explored the effects on crystal packing morphology for the indeno[1,2-b]fluorene...

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Detalles Bibliográficos
Autores principales: Rose, Bradley D, Santa Maria, Peter J, Fix, Aaron G, Vonnegut, Chris L, Zakharov, Lev N, Parkin, Sean R, Haley, Michael M
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2014
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4168888/
https://www.ncbi.nlm.nih.gov/pubmed/25246970
http://dx.doi.org/10.3762/bjoc.10.219