Crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone

The structure of the title compound, C(10)H(11)N(3)OS, comprises an approximately planar mol­ecule, with the r.m.s. deviation for the 15 non-H atoms being 0.089 Å. The conformation about the imine bond is E and an intra­molecular N—H⋯N hydrogen bond is evident. Mol­ecules are linked into a supra­mol...

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Autores principales: Pino-Cuevas, Arantxa, Carballo, Rosa, Vázquez-López, Ezequiel M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186068/
https://www.ncbi.nlm.nih.gov/pubmed/25309257
http://dx.doi.org/10.1107/S1600536814016407
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author Pino-Cuevas, Arantxa
Carballo, Rosa
Vázquez-López, Ezequiel M.
author_facet Pino-Cuevas, Arantxa
Carballo, Rosa
Vázquez-López, Ezequiel M.
author_sort Pino-Cuevas, Arantxa
collection PubMed
description The structure of the title compound, C(10)H(11)N(3)OS, comprises an approximately planar mol­ecule, with the r.m.s. deviation for the 15 non-H atoms being 0.089 Å. The conformation about the imine bond is E and an intra­molecular N—H⋯N hydrogen bond is evident. Mol­ecules are linked into a supra­molecular chain along the b axis by N—H⋯S hydrogen bonds.
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spelling pubmed-41860682014-10-12 Crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone Pino-Cuevas, Arantxa Carballo, Rosa Vázquez-López, Ezequiel M. Acta Crystallogr Sect E Struct Rep Online Data Reports The structure of the title compound, C(10)H(11)N(3)OS, comprises an approximately planar mol­ecule, with the r.m.s. deviation for the 15 non-H atoms being 0.089 Å. The conformation about the imine bond is E and an intra­molecular N—H⋯N hydrogen bond is evident. Mol­ecules are linked into a supra­molecular chain along the b axis by N—H⋯S hydrogen bonds. International Union of Crystallography 2014-08-01 /pmc/articles/PMC4186068/ /pubmed/25309257 http://dx.doi.org/10.1107/S1600536814016407 Text en © Pino-Cuevas et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Pino-Cuevas, Arantxa
Carballo, Rosa
Vázquez-López, Ezequiel M.
Crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone
title Crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone
title_full Crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone
title_fullStr Crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone
title_full_unstemmed Crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone
title_short Crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone
title_sort crystal structure of 1-(4-formyl­benzyl­idene)-4-methyl­thio­semicarbazone
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186068/
https://www.ncbi.nlm.nih.gov/pubmed/25309257
http://dx.doi.org/10.1107/S1600536814016407
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