Crystal structure of ethyl (E)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate

In the title compound, C(13)H(13)ClO(4), the dihedral angle between the chloro­benezene ring and the least-squares plane through the 4-meth­oxy-2-oxobut-3-enoate ethyl ester residue (r.m.s. deviation = 0.0975 Å) is 54.10 (5)°. In the crystal, mol­ecules are connected by meth­oxy–ketone and benzene–c...

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Autores principales: Flores, Darlene Correia, Vicenti, Juliano Rosa de Menezes, Pereira, Bruna Ávila, da Silva, Gabriele Marques Dias, Zambiazi, Priscilla Jussiane
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186072/
https://www.ncbi.nlm.nih.gov/pubmed/25309205
http://dx.doi.org/10.1107/S1600536814017280
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author Flores, Darlene Correia
Vicenti, Juliano Rosa de Menezes
Pereira, Bruna Ávila
da Silva, Gabriele Marques Dias
Zambiazi, Priscilla Jussiane
author_facet Flores, Darlene Correia
Vicenti, Juliano Rosa de Menezes
Pereira, Bruna Ávila
da Silva, Gabriele Marques Dias
Zambiazi, Priscilla Jussiane
author_sort Flores, Darlene Correia
collection PubMed
description In the title compound, C(13)H(13)ClO(4), the dihedral angle between the chloro­benezene ring and the least-squares plane through the 4-meth­oxy-2-oxobut-3-enoate ethyl ester residue (r.m.s. deviation = 0.0975 Å) is 54.10 (5)°. In the crystal, mol­ecules are connected by meth­oxy–ketone and benzene–carboxyl­ate carbonyl C—H⋯O inter­actions, generating a supra­molecular layer in the ac plane.
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spelling pubmed-41860722014-10-12 Crystal structure of ethyl (E)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate Flores, Darlene Correia Vicenti, Juliano Rosa de Menezes Pereira, Bruna Ávila da Silva, Gabriele Marques Dias Zambiazi, Priscilla Jussiane Acta Crystallogr Sect E Struct Rep Online Data Reports In the title compound, C(13)H(13)ClO(4), the dihedral angle between the chloro­benezene ring and the least-squares plane through the 4-meth­oxy-2-oxobut-3-enoate ethyl ester residue (r.m.s. deviation = 0.0975 Å) is 54.10 (5)°. In the crystal, mol­ecules are connected by meth­oxy–ketone and benzene–carboxyl­ate carbonyl C—H⋯O inter­actions, generating a supra­molecular layer in the ac plane. International Union of Crystallography 2014-08-16 /pmc/articles/PMC4186072/ /pubmed/25309205 http://dx.doi.org/10.1107/S1600536814017280 Text en © Flores et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Flores, Darlene Correia
Vicenti, Juliano Rosa de Menezes
Pereira, Bruna Ávila
da Silva, Gabriele Marques Dias
Zambiazi, Priscilla Jussiane
Crystal structure of ethyl (E)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate
title Crystal structure of ethyl (E)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate
title_full Crystal structure of ethyl (E)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate
title_fullStr Crystal structure of ethyl (E)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate
title_full_unstemmed Crystal structure of ethyl (E)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate
title_short Crystal structure of ethyl (E)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate
title_sort crystal structure of ethyl (e)-4-(4-chlorophen­yl)-4-meth­oxy-2-oxobut-3-enoate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186072/
https://www.ncbi.nlm.nih.gov/pubmed/25309205
http://dx.doi.org/10.1107/S1600536814017280
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