Crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl N,N-diiso­propyl­dithio­carbamate

In the title compound, C(17)H(27)N(3)OS(2), the amide group is approximately coplanar with the pyridine ring [dihedral angle = 1.6 (1)°], whereas the di­thio­carbamate group is nearly perpendicular to the pyridine ring [dihedral angle = 76.7 (1)°]. In the crystal, pairs of weak C—H⋯O hydrogen bonds...

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Detalles Bibliográficos
Autores principales: El-Hiti, Gamal A., Smith, Keith, Hegazy, Amany S., Baashen, Mohammed, Kariuki, Benson M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186077/
https://www.ncbi.nlm.nih.gov/pubmed/25309230
http://dx.doi.org/10.1107/S1600536814019321
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author El-Hiti, Gamal A.
Smith, Keith
Hegazy, Amany S.
Baashen, Mohammed
Kariuki, Benson M.
author_facet El-Hiti, Gamal A.
Smith, Keith
Hegazy, Amany S.
Baashen, Mohammed
Kariuki, Benson M.
author_sort El-Hiti, Gamal A.
collection PubMed
description In the title compound, C(17)H(27)N(3)OS(2), the amide group is approximately coplanar with the pyridine ring [dihedral angle = 1.6 (1)°], whereas the di­thio­carbamate group is nearly perpendicular to the pyridine ring [dihedral angle = 76.7 (1)°]. In the crystal, pairs of weak C—H⋯O hydrogen bonds link the mol­ecules into inversion dimers.
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spelling pubmed-41860772014-10-12 Crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl N,N-diiso­propyl­dithio­carbamate El-Hiti, Gamal A. Smith, Keith Hegazy, Amany S. Baashen, Mohammed Kariuki, Benson M. Acta Crystallogr Sect E Struct Rep Online Data Reports In the title compound, C(17)H(27)N(3)OS(2), the amide group is approximately coplanar with the pyridine ring [dihedral angle = 1.6 (1)°], whereas the di­thio­carbamate group is nearly perpendicular to the pyridine ring [dihedral angle = 76.7 (1)°]. In the crystal, pairs of weak C—H⋯O hydrogen bonds link the mol­ecules into inversion dimers. International Union of Crystallography 2014-08-30 /pmc/articles/PMC4186077/ /pubmed/25309230 http://dx.doi.org/10.1107/S1600536814019321 Text en © El-Hiti et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
El-Hiti, Gamal A.
Smith, Keith
Hegazy, Amany S.
Baashen, Mohammed
Kariuki, Benson M.
Crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl N,N-diiso­propyl­dithio­carbamate
title Crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl N,N-diiso­propyl­dithio­carbamate
title_full Crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl N,N-diiso­propyl­dithio­carbamate
title_fullStr Crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl N,N-diiso­propyl­dithio­carbamate
title_full_unstemmed Crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl N,N-diiso­propyl­dithio­carbamate
title_short Crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl N,N-diiso­propyl­dithio­carbamate
title_sort crystal structure of 4-(2,2-di­methyl­propanamido)­pyridin-3-yl n,n-diiso­propyl­dithio­carbamate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186077/
https://www.ncbi.nlm.nih.gov/pubmed/25309230
http://dx.doi.org/10.1107/S1600536814019321
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