Crystal structure of (E)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine

The title compound, C(19)H(15)N(3)O(2), shows an E conformation of the imine bond. The dihedral angle between the planes of the phenyl rings in the di­phenyl­hydrazine groups is 88.52 (4)°. The 2-nitro­benzene ring shows a torsion angle of 10.17 (8)° with the C=N—N plane. A short intra­molecular C—H...

Descripción completa

Detalles Bibliográficos
Autores principales: Flores-Alamo, Marcos, Meléndrez-Luévano, Ruth, Ortiz Márquez, José A., Sansinenea Royano, Estibaliz, Cabrera-Vivas, Blanca M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186103/
https://www.ncbi.nlm.nih.gov/pubmed/25309247
http://dx.doi.org/10.1107/S1600536814016109
_version_ 1782337997171064832
author Flores-Alamo, Marcos
Meléndrez-Luévano, Ruth
Ortiz Márquez, José A.
Sansinenea Royano, Estibaliz
Cabrera-Vivas, Blanca M.
author_facet Flores-Alamo, Marcos
Meléndrez-Luévano, Ruth
Ortiz Márquez, José A.
Sansinenea Royano, Estibaliz
Cabrera-Vivas, Blanca M.
author_sort Flores-Alamo, Marcos
collection PubMed
description The title compound, C(19)H(15)N(3)O(2), shows an E conformation of the imine bond. The dihedral angle between the planes of the phenyl rings in the di­phenyl­hydrazine groups is 88.52 (4)°. The 2-nitro­benzene ring shows a torsion angle of 10.17 (8)° with the C=N—N plane. A short intra­molecular C—H⋯O contact occurs. In the crystal, only van der Waals contacts occur between the mol­ecules.
format Online
Article
Text
id pubmed-4186103
institution National Center for Biotechnology Information
language English
publishDate 2014
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-41861032014-10-12 Crystal structure of (E)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine Flores-Alamo, Marcos Meléndrez-Luévano, Ruth Ortiz Márquez, José A. Sansinenea Royano, Estibaliz Cabrera-Vivas, Blanca M. Acta Crystallogr Sect E Struct Rep Online Data Reports The title compound, C(19)H(15)N(3)O(2), shows an E conformation of the imine bond. The dihedral angle between the planes of the phenyl rings in the di­phenyl­hydrazine groups is 88.52 (4)°. The 2-nitro­benzene ring shows a torsion angle of 10.17 (8)° with the C=N—N plane. A short intra­molecular C—H⋯O contact occurs. In the crystal, only van der Waals contacts occur between the mol­ecules. International Union of Crystallography 2014-08-01 /pmc/articles/PMC4186103/ /pubmed/25309247 http://dx.doi.org/10.1107/S1600536814016109 Text en © Flores-Alamo et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Flores-Alamo, Marcos
Meléndrez-Luévano, Ruth
Ortiz Márquez, José A.
Sansinenea Royano, Estibaliz
Cabrera-Vivas, Blanca M.
Crystal structure of (E)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine
title Crystal structure of (E)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine
title_full Crystal structure of (E)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine
title_fullStr Crystal structure of (E)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine
title_full_unstemmed Crystal structure of (E)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine
title_short Crystal structure of (E)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine
title_sort crystal structure of (e)-1-(2-nitro­benzyl­idene)-2,2-di­phenyl­hydrazine
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186103/
https://www.ncbi.nlm.nih.gov/pubmed/25309247
http://dx.doi.org/10.1107/S1600536814016109
work_keys_str_mv AT floresalamomarcos crystalstructureofe12nitrobenzylidene22diphenylhydrazine
AT melendrezluevanoruth crystalstructureofe12nitrobenzylidene22diphenylhydrazine
AT ortizmarquezjosea crystalstructureofe12nitrobenzylidene22diphenylhydrazine
AT sansinenearoyanoestibaliz crystalstructureofe12nitrobenzylidene22diphenylhydrazine
AT cabreravivasblancam crystalstructureofe12nitrobenzylidene22diphenylhydrazine

Ejemplares similares