Crystal structure of N-(1-allyl-3-chloro-4-eth­oxy-1H-indazol-5-yl)-4-meth­oxybenzene­sulfonamide

In the title compound, C(19)H(20)ClN(3)O(4)S, the benzene ring is inclined to the indazole ring system (r.m.s. deviation = 0.014 Å) by 65.07 (8)°. The allyl and eth­oxy groups are almost normal to the indazole ring, as indicated by the respective torsion angles [N—N—C—C = 111.6 (2) and C—C—O—C = −88...

Descripción completa

Detalles Bibliográficos
Autores principales: Chicha, Hakima, Rakib, El Mostapha, Bouissane, Latifa, Saadi, Mohamed, El Ammari, Lahcen
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186176/
https://www.ncbi.nlm.nih.gov/pubmed/25309208
http://dx.doi.org/10.1107/S1600536814018492
_version_ 1782338014302699520
author Chicha, Hakima
Rakib, El Mostapha
Bouissane, Latifa
Saadi, Mohamed
El Ammari, Lahcen
author_facet Chicha, Hakima
Rakib, El Mostapha
Bouissane, Latifa
Saadi, Mohamed
El Ammari, Lahcen
author_sort Chicha, Hakima
collection PubMed
description In the title compound, C(19)H(20)ClN(3)O(4)S, the benzene ring is inclined to the indazole ring system (r.m.s. deviation = 0.014 Å) by 65.07 (8)°. The allyl and eth­oxy groups are almost normal to the indazole ring, as indicated by the respective torsion angles [N—N—C—C = 111.6 (2) and C—C—O—C = −88.1 (2)°]. In the crystal, mol­ecules are connected by N—H⋯N hydrogen bonds, forming helical chains propagating along [010]. The chains are linked by C—H⋯O hydrogen bonds, forming a three-dimensional network.
format Online
Article
Text
id pubmed-4186176
institution National Center for Biotechnology Information
language English
publishDate 2014
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-41861762014-10-12 Crystal structure of N-(1-allyl-3-chloro-4-eth­oxy-1H-indazol-5-yl)-4-meth­oxybenzene­sulfonamide Chicha, Hakima Rakib, El Mostapha Bouissane, Latifa Saadi, Mohamed El Ammari, Lahcen Acta Crystallogr Sect E Struct Rep Online Data Reports In the title compound, C(19)H(20)ClN(3)O(4)S, the benzene ring is inclined to the indazole ring system (r.m.s. deviation = 0.014 Å) by 65.07 (8)°. The allyl and eth­oxy groups are almost normal to the indazole ring, as indicated by the respective torsion angles [N—N—C—C = 111.6 (2) and C—C—O—C = −88.1 (2)°]. In the crystal, mol­ecules are connected by N—H⋯N hydrogen bonds, forming helical chains propagating along [010]. The chains are linked by C—H⋯O hydrogen bonds, forming a three-dimensional network. International Union of Crystallography 2014-08-20 /pmc/articles/PMC4186176/ /pubmed/25309208 http://dx.doi.org/10.1107/S1600536814018492 Text en © Chicha et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Chicha, Hakima
Rakib, El Mostapha
Bouissane, Latifa
Saadi, Mohamed
El Ammari, Lahcen
Crystal structure of N-(1-allyl-3-chloro-4-eth­oxy-1H-indazol-5-yl)-4-meth­oxybenzene­sulfonamide
title Crystal structure of N-(1-allyl-3-chloro-4-eth­oxy-1H-indazol-5-yl)-4-meth­oxybenzene­sulfonamide
title_full Crystal structure of N-(1-allyl-3-chloro-4-eth­oxy-1H-indazol-5-yl)-4-meth­oxybenzene­sulfonamide
title_fullStr Crystal structure of N-(1-allyl-3-chloro-4-eth­oxy-1H-indazol-5-yl)-4-meth­oxybenzene­sulfonamide
title_full_unstemmed Crystal structure of N-(1-allyl-3-chloro-4-eth­oxy-1H-indazol-5-yl)-4-meth­oxybenzene­sulfonamide
title_short Crystal structure of N-(1-allyl-3-chloro-4-eth­oxy-1H-indazol-5-yl)-4-meth­oxybenzene­sulfonamide
title_sort crystal structure of n-(1-allyl-3-chloro-4-eth­oxy-1h-indazol-5-yl)-4-meth­oxybenzene­sulfonamide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186176/
https://www.ncbi.nlm.nih.gov/pubmed/25309208
http://dx.doi.org/10.1107/S1600536814018492
work_keys_str_mv AT chichahakima crystalstructureofn1allyl3chloro4ethoxy1hindazol5yl4methoxybenzenesulfonamide
AT rakibelmostapha crystalstructureofn1allyl3chloro4ethoxy1hindazol5yl4methoxybenzenesulfonamide
AT bouissanelatifa crystalstructureofn1allyl3chloro4ethoxy1hindazol5yl4methoxybenzenesulfonamide
AT saadimohamed crystalstructureofn1allyl3chloro4ethoxy1hindazol5yl4methoxybenzenesulfonamide
AT elammarilahcen crystalstructureofn1allyl3chloro4ethoxy1hindazol5yl4methoxybenzenesulfonamide

Ejemplares similares