Crystal structure of (3R)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid

The characteristic feature of the title mol­ecule, C(16)H(23)NO(4), is the syn configuration of the partially double amide C—N bond [C—N—C—O torsion angle = −14.8 (2)°]. The crystal packing is determined by inter­molecular O—H⋯O and N—H⋯O hydrogen bonds, which link the mol­ecules into a double-chain...

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Detalles Bibliográficos
Autores principales: Jędrzejczak, Karol, Szczesio, Małgorzata, Oracz, Monika, Jankowski, Stefan, Główka, Marek L.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257155/
https://www.ncbi.nlm.nih.gov/pubmed/25484683
http://dx.doi.org/10.1107/S1600536814019497
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author Jędrzejczak, Karol
Szczesio, Małgorzata
Oracz, Monika
Jankowski, Stefan
Główka, Marek L.
author_facet Jędrzejczak, Karol
Szczesio, Małgorzata
Oracz, Monika
Jankowski, Stefan
Główka, Marek L.
author_sort Jędrzejczak, Karol
collection PubMed
description The characteristic feature of the title mol­ecule, C(16)H(23)NO(4), is the syn configuration of the partially double amide C—N bond [C—N—C—O torsion angle = −14.8 (2)°]. The crystal packing is determined by inter­molecular O—H⋯O and N—H⋯O hydrogen bonds, which link the mol­ecules into a double-chain structure extending along [010].
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spelling pubmed-42571552014-12-05 Crystal structure of (3R)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid Jędrzejczak, Karol Szczesio, Małgorzata Oracz, Monika Jankowski, Stefan Główka, Marek L. Acta Crystallogr Sect E Struct Rep Online Data Reports The characteristic feature of the title mol­ecule, C(16)H(23)NO(4), is the syn configuration of the partially double amide C—N bond [C—N—C—O torsion angle = −14.8 (2)°]. The crystal packing is determined by inter­molecular O—H⋯O and N—H⋯O hydrogen bonds, which link the mol­ecules into a double-chain structure extending along [010]. International Union of Crystallography 2014-09-03 /pmc/articles/PMC4257155/ /pubmed/25484683 http://dx.doi.org/10.1107/S1600536814019497 Text en © Jędrzejczak et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Jędrzejczak, Karol
Szczesio, Małgorzata
Oracz, Monika
Jankowski, Stefan
Główka, Marek L.
Crystal structure of (3R)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid
title Crystal structure of (3R)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid
title_full Crystal structure of (3R)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid
title_fullStr Crystal structure of (3R)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid
title_full_unstemmed Crystal structure of (3R)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid
title_short Crystal structure of (3R)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid
title_sort crystal structure of (3r)-3-benzyl-4-[(tert-but­oxy­carbon­yl)amino]­butanoic acid
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257155/
https://www.ncbi.nlm.nih.gov/pubmed/25484683
http://dx.doi.org/10.1107/S1600536814019497
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