Crystal structure of (Z)-2-hy­droxy-N′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide

In the title compound, C(10)H(9)N(3)O(3)S, the five-membered ring adopts a slightly twisted conformation about the C(m)—S (m = methyl­ene) bond. The dihedral angle between this ring and the benzene ring is 7.99 (9)°. A bifurcated intra­molecular N—H⋯(O,S) hydrogen bond helps to establish the near pl...

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Detalles Bibliográficos
Autores principales: Zhang, Ya, Li, Peijuan, Fan, Xin, Jin, Longfei
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257235/
https://www.ncbi.nlm.nih.gov/pubmed/25484807
http://dx.doi.org/10.1107/S1600536814022351
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author Zhang, Ya
Li, Peijuan
Fan, Xin
Jin, Longfei
author_facet Zhang, Ya
Li, Peijuan
Fan, Xin
Jin, Longfei
author_sort Zhang, Ya
collection PubMed
description In the title compound, C(10)H(9)N(3)O(3)S, the five-membered ring adopts a slightly twisted conformation about the C(m)—S (m = methyl­ene) bond. The dihedral angle between this ring and the benzene ring is 7.99 (9)°. A bifurcated intra­molecular N—H⋯(O,S) hydrogen bond helps to establish the near planar conformation of the mol­ecule. In the crystal, mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen bonds to generate (001) sheets.
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spelling pubmed-42572352014-12-05 Crystal structure of (Z)-2-hy­droxy-N′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide Zhang, Ya Li, Peijuan Fan, Xin Jin, Longfei Acta Crystallogr Sect E Struct Rep Online Data Reports In the title compound, C(10)H(9)N(3)O(3)S, the five-membered ring adopts a slightly twisted conformation about the C(m)—S (m = methyl­ene) bond. The dihedral angle between this ring and the benzene ring is 7.99 (9)°. A bifurcated intra­molecular N—H⋯(O,S) hydrogen bond helps to establish the near planar conformation of the mol­ecule. In the crystal, mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen bonds to generate (001) sheets. International Union of Crystallography 2014-10-18 /pmc/articles/PMC4257235/ /pubmed/25484807 http://dx.doi.org/10.1107/S1600536814022351 Text en © Zhang et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Zhang, Ya
Li, Peijuan
Fan, Xin
Jin, Longfei
Crystal structure of (Z)-2-hy­droxy-N′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide
title Crystal structure of (Z)-2-hy­droxy-N′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide
title_full Crystal structure of (Z)-2-hy­droxy-N′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide
title_fullStr Crystal structure of (Z)-2-hy­droxy-N′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide
title_full_unstemmed Crystal structure of (Z)-2-hy­droxy-N′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide
title_short Crystal structure of (Z)-2-hy­droxy-N′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide
title_sort crystal structure of (z)-2-hy­droxy-n′-(4-oxo-1,3-thia­zolidin-2-yl­idene)benzohydrazide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257235/
https://www.ncbi.nlm.nih.gov/pubmed/25484807
http://dx.doi.org/10.1107/S1600536814022351
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